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Validation of ICP-MS method for trace level analysis of Pb in plasma
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  • Journal title : Analytical Science and Technology
  • Volume 28, Issue 5,  2015, pp.309-316
  • Publisher : The Korean Society of Analytical Science
  • DOI : 10.5806/AST.2015.28.5.309
 Title & Authors
Validation of ICP-MS method for trace level analysis of Pb in plasma
Lee, Sung-Bae; Kim, Yong-Soon; Lee, Yong-Hoon; Ahn, Byung-Joon; Kim, Nam-Soo; Lee, Byung-Kook; Shin, Ho-Sang;
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 Abstract
The analytical method of lead in plasma by ICP-MS was validated after securing environment within class 1,000 classification. We tested specificity and accuracy of within-run and between-run. According to measurement of the amount of suspended particulates in a clean room, 0.3~62 particles were detected in 0.3 µm size while 0.0~28.3 particles were observed in 0.5 µm size. Total suspended particulates met required environment with up to 90.3 particles. The MDL (Method detection limit) of the sample which has been fabricated using fetal bovine serum (FBS) blank was 1.77 ng/L, and LOQ (Limit of quantification) was 5.55 ng/L. The slope, intercept and correlation coefficient of the calibration curve were y
 Keywords
validation;lead;plasma;inductively coupled plasma-mass spectrometry;
 Language
Korean
 Cited by
 References
1.
B. K. Lee, J. J. Kim, K. H. Woo and H. S. Kim, Health Care Technology Research and Development Annual Report, Ministry of Health and Human Services, 2002.

2.
H. Hu, M. Rabinowitz and D. Smith, Environ. Health Perspect., 106(1), 1-8 (1998). crossref(new window)

3.
R. Cornelis, B. Heinzow, R. F. M. Herber, J. Molin Christensen, O. M. Paulsen, E. Sabbioni, D. M. Templeton, Y. Thomassen, M. Vahter, and O. Vesterberg, Pure & Appl. Chem., 67 (Nos 8/9), 1575-1608 (1995).

4.
J.-W. Choi, N.-S. Kim, K.-S. Cho, J.-O Ham and B.-K. Lee, J. Korea Soc. Occup. Environ. Hyg., 20(1), 10-18 (2010).

5.
Korea Occupational Safety & Health Agency (KOSHA), Industrial Accident Statistics, http://eip.kosha.or.kr/jsp/Main.jsp?On=OPEN, Assessed 29 Oct 2014.

6.
M. M. Telléz-Rojo, M. Hernández-Avila,H. Lamadridfigueroa, D. Smith, L. Hernández-Cadena, A. Mercado, A. Aro, J. Schwartz and H. Hu, American J. Epidemiology, 160, 668-678 (2004). crossref(new window)

7.
F. Barbosa Jr., I. Ramires, M. H. C. Rodrigues, T. D. Saint’ Pierre, A. J. Curtius, M. R. Buzalaf, R. F. Gerlach and J. E. Tanus-Santos, Environ. Res., 102, 90-95 (2006). crossref(new window)

8.
M. Hernández-Avila, D. Smith, F. Meneses, R et al., Environ. Health Perspect., 106(8), 473-477 (1998). crossref(new window)

9.
F. J. Roberts, L. Ebdon and S. J. Hill, J. Trace Elements Med. Biol. 14, 108-115 (2000). crossref(new window)

10.
S. S. Choi, and S. H. Lee, J. Korean Soc. Environ. Adm., 8(4), 331-337 (2002).

11.
G. R. C. Almeida, C. F. Freitas Tavares, A. M. Souza, T. S. Sousa, C. A. R. Funayama, F. Barbosa Jr., J. E. Tanus-Santos and R. F. Gerlach, Sci. Total Environ., 408, 1551-1556 (2010). crossref(new window)

12.
G. A. K. Koyashiki, M. M. B. Paoliello, T. Matsuo, M. M. B. Oliveira, L. Mezzaroba, M. Fátima Carvalho, A. M. Sakuma, C. Turini, M. T. O. Vannuchi, and C. S. D. Barbosa, Environ. Res., 110, 265-271 (2010). crossref(new window)

13.
S.-B. Lee, J.-S. Yang, S.-B. Choi and H.-S. Shin, Anal. Sci. Technol., 25(3), 190-196 (2012). crossref(new window)

14.
S.-B. Lee, J.-S. Yang, S.-B. Choi, N.-S. Kim, B.-K. Lee and H.-S. Shin, J. Korean Soc. Occup. Environ. Hyg., 23(2), 65-74 (2013).

15.
M. F. Montenegro, F. Barbosa Jr., V. C. Sandrim, R. F. Gerlach, J. E. Tanus-Santos, Arch Toxicol., 80, 394-398 (2006). crossref(new window)

16.
V. B. Rezende, J. H. Amaral, R. F. Gerlach, F. barbosa Jr., and J. E. Tanus-Santos, J. Trace Elem. Med. Biol., 24, 147-151 (2010). crossref(new window)

17.
K. S. Park and S. T. Kim, Anal. Sci. Technol., 10(4), 240-245 (1997).

18.
F. Barbosa Jr., J. E. Tanus-Santos, R. F. Gerhach and P. J. Parsons, Environ. Health Perspect., 113(12), 1669-1674 (2005). crossref(new window)

19.
Ministry of Food and Drug Safety, Guideline for the Validation of Bioanalytical Method, 2010.

20.
I. A. Bergdahl, L. Gerhardsson, I. E. Liljelind, L Nilsson and S. Skerfving, Am. J. Ind. Med., 49, 93-101 (2006). crossref(new window)

21.
N.-S. Kim, J.-H. Kim, B.-K. Jang, H.-S. Kim, K.-D. Ahn and B.-K. Lee, J. Korean Soc. Occup. Environ Hyg., 17(1), 43-52 (2007).

22.
M. F. Montenegro, F. Barbosa Jr, V. C. Sandrim, R. F. Gerlach and J. E. Tanus-Santos, Arch Toxicol., 80, 394-398 (2006). crossref(new window)

23.
C. D. Palmer, M. E. Lewis Jr., C. M. Geraghty, F. Barbosa Jr., and P. J. Parsons, Spectrochim. Acta B, 61, 980-990 (2006). crossref(new window)

24.
N.-S. Kim, K-S. Jung and B.-K. Lee, J. Korean Soc. Occup. Environ. Hyg., 21(4), 193-200 (2011).

25.
K. S. Park and S. T. Kim, Anal. Sci. Technol., 10(4), 240-245 (1997).

26.
D. Smith, M. Hernandez-Avila, M. M. Téllez Rojo, A. Merado and H. Hu, Environ. Health Perspect., 110(3), 263-268 (2002). crossref(new window)

27.
J. A. Nunes, B. L. Batista, J. L. Rodrigues, N. M. Caldas, J. A. Neto, and F. Barbosa Jr, J. Toxicol. Environ. Health A,. 73(13-14), 878-887 (2010). crossref(new window)

28.
G. R. Almeida, C. F. Freitas Tavares, A. M. Souza, T. S. Sousa, C. A. R. Funayma, F. Barbosa Jr, J. E. TnusSantos, and R. F. Gerlach, Sci. Total Environ., 408, 1551-1556 (2010). crossref(new window)

29.
E. Bárány, I. A. Bergdahl, L.-E. Bratteby, T. Lundh, G. Samuelson, A. Schütz, S. Skerfving and A. Oskarsson, Sci. Total Environ., 286, 129-141 (2002). crossref(new window)

30.
A. Schütz, I. A. Bergdahl, A. Ekhom and S. Skerfving, Occup. Environ. Med., 53, 736-740 (1996). crossref(new window)

31.
I. A. Bergdahl, A. Schütz, L. Gerhardsson, A. Jensen and S. Skerfving, Scand. J. Work Environ. Health, 23(5), 359-363 (1997). crossref(new window)

32.
I. A. Bergdahl, M. Vahter, S. A. Counter, A. Schütz, L. H. Buchanan, F. Ortega, G. Laurell and S. Skerfving, Environ. Res. Sect. A, 80, 25-33 (1999). crossref(new window)