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Introduction of the Rapid Analysis Method for PCBs in Insulating Oils and Its Comparison Study to the Analysis Method in Korea
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  • Journal title : Environmental Engineering Research
  • Volume 16, Issue 1,  2011, pp.11-18
  • Publisher : Korean Society of Environmental Engineering
  • DOI : 10.4491/eer.2011.16.1.011
 Title & Authors
Introduction of the Rapid Analysis Method for PCBs in Insulating Oils and Its Comparison Study to the Analysis Method in Korea
Hong, Jang-Ho; Takahashi, Tomohumi; Ishizaka, Takahiro; Toita, Hideki; Min, Byung-Yoon; Honda, Katsuhisa;
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 Abstract
The aim of this research was to introduce a new rapid analysis method (heating of the multi-layer silica gel column/alumina column) for polychlorinated biphenyls in insulating oils, and to compare our new method with the analytical method currently used in Korea. The entire pretreatment procedure was completed within 2 hr, using about only 20 mL of solvents via our rapid analytical method. Furthermore, the pretreatment procedure can always be uniformly performed, regardless of oil type (JIS 1~JIS 7 and KS 1~KS 7). The recovery rates were more than 89%, with relative standard deviations below 6.0%. In conclusion, this rapid analytical method could reduce the pretreatment time and solvent usage by 1/10 and between 1/25 and 1/50, respectively, compared to analytical method currently used in Korea.
 Keywords
Insulating oils;Polychlorinated biphenyls;Rapid analysis;
 Language
English
 Cited by
1.
카트리지 전처리를 이용한 절연유 중 PCBs 동족체의 정확도 평가,임태숙;정인영;김지인;고상호;이원석;

한국환경분석학회지, 2013. vol.16. 3, pp.220-228
1.
Dechlorination and decomposition of Aroclor 1242 in real waste transformer oil using a nucleophilic material with a modified domestic microwave oven, Journal of Material Cycles and Waste Management, 2014, 16, 4, 711  crossref(new windwow)
2.
Screening of polychlorinated biphenyls in insulating oil using a microfluidic based pretreatment and immunoassay, Analytical Chemistry Research, 2015, 3, 13  crossref(new windwow)
3.
Development of the automated cleanup system for the analysis of PCDDs, PCDFs and DL-PCBs, Chemosphere, 2012, 88, 11, 1287  crossref(new windwow)
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