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Validation of Bulk Analysis with Simulated Swipe Samples Containing Ultra-Trace Amounts of Uranium and Plutonium Using MC-ICP-MS
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  • Journal title : Mass Spectrometry Letters
  • Volume 6, Issue 3,  2015, pp.75-79
  • Publisher : Korean Society Mass Spectrometry
  • DOI : 10.5478/MSL.2015.6.3.75
 Title & Authors
Validation of Bulk Analysis with Simulated Swipe Samples Containing Ultra-Trace Amounts of Uranium and Plutonium Using MC-ICP-MS
Lim, Sang Ho; Han, Sun-Ho; Park, Jong-Ho; Park, Ranhee; Lee, Min Young; Park, Jinkyu; Lee, Chi-Gyu; Song, Kyuseok;
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 Abstract
Suitable analytical procedures for the bulk analysis of ultra-trace amounts of uranium and plutonium have been developed using multi-collector inductively coupled mass spectrometry (MC-ICP-MS). The quantification and determination of the isotopic ratios of uranium and plutonium in three simulated swipe samples, a swipe blank, and a process blank were performed to validate the analytical performance. The analytical results for the simulated swipe samples were in good agreement with the certified values, based on the measurement quality goals for the analysis of bulk environmental samples recommended by the International Atomic Energy Agency (IAEA)
 Keywords
Bulk analysis;Environmental samples;Chemical separation;IDMS;MC-ICP-MS;
 Language
English
 Cited by
1.
Recent Developments in Nuclear Forensic and Nuclear Safeguards Analysis Using Mass Spectrometry, Mass Spectrometry Letters, 2016, 7, 2, 31  crossref(new windwow)
2.
Uranium isotope analysis by MC-ICP-MS in sub-ng sized samples, J. Anal. At. Spectrom., 2016, 31, 11, 2272  crossref(new windwow)
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