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Monitoring for cephalosporins residues in raw meat in Seoul
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 Title & Authors
Monitoring for cephalosporins residues in raw meat in Seoul
Kim, Mi-Ran; Choi, Yoon-Hwa; Choi, Hoon; Kim, Doo-Hwan; Kim, Young-Seob; Lee, Ju-Hyung;
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We investigated the residues of 6 cephalosporins (cefquinome, cephalexin, cephalonium, cefazolin, ceftiofur, cefuroxime) using LC-MS/MS in raw meat in Seoul. This method involves extraction of the residue from the meat by distilled water and methanol followed by a manual of residue analysis published by the National Institute of Food and Drug Safety Evaluation. The recoveries ranged between 74.71~90.01% in beef, 73.37~101.40% in pork and 70.87~95.53% in chicken, respectively. The limits of detection were 0.0004~0.0563 mg/kg, and the limits of quantification were 0.001~0.169 mg/kg respectively. Residues of cephalosporins which exceeded maximum residue limits (MRL) were not exceed in any of the 287 samples. However, it is necessary to develop multi-method, which includes the active metabolites of ceftiofur.
Cephalosporins residues;Raw meat;LC-MS/MS;
 Cited by
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