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Multiresidue Analysis Method for Determination of Unregistered Organophosphorus Pesticides in Korea for Imported Agri-Food
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 Title & Authors
Multiresidue Analysis Method for Determination of Unregistered Organophosphorus Pesticides in Korea for Imported Agri-Food
Jeon, Young-Hwan; Hwang, Jeong-In; Ahn, Ji-Woon; Kim, Hyo-Young; Do, Jung-Ah; Oh, Jae-Ho; Hwang, In-Gyun; Im, Moo-Hyeog; Lee, Joong-Keun; Lee, Young-Deuk; Kim, Jang-Eok;
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 Abstract
BACKGROUND: For safety evaluation of imported agri-food in Korea, the multiresidue analysis method was establised for unregistered organophosphorus pesticides, aspon, chlorthion, chlorthiophos, crotoxyphos, demeton-O, demeton-S, demeton-S-methyl, dioxathion, heptenophos, iodofenphos, leptophos, methyl-trithion, propetamphos and sulfotep. METHODS AND RESULTS: The used method for multiresidue analysis in brown rice and orange used as representative samples of imported agri-food was the official method of Korean Food and Drug Administration. The results of validation test of 13 organophosphorus pesticides except crotoxyphos for multiresidue analysis method are compared to the criteria such as specificity, linearity, accuracy, precision and limit of quantification. CONCLUSION: The used method for multiresidue analysis of unregistered 13 organophosphorus pesticides except crotoxyphos in Korea can surely be used as an official method for routine analysis of imported agri-food.
 Keywords
Imported agri-food;Multiresidue analysis;Unregistered organophosphorus pesticides;Validation test;
 Language
Korean
 Cited by
1.
콩고민주공화국의 킨샤사 사질 밭에서 벼 농림나1호의 생육특성,강위금;이성희;한준호;구총림;이상호;유소라;양창인;김민태;류진희;김현순;

한국국제농업개발학회지, 2014. vol.26. 4, pp.365-371 crossref(new window)
2.
가스 크로마토그래피를 이용한 수입농산물 중 국내 미등록 농약의 다성분 동시분석법 적용,이지원;강정균;권혜영;노진호;진용덕;이제봉;홍수명;김택겸;조남준;

농약과학회지, 2015. vol.19. 3, pp.161-173 crossref(new window)
1.
Gas Chromatographic Method for Multiresidue Analysis of Unregistered Pesticides in Imported Agricultural Commodities, The Korean Journal of Pesticide Science, 2015, 19, 3, 161  crossref(new windwow)
 References
1.
Borras, E., Sanchez, P., Munoz, A., Tortajada-Genaro L.A., 2011. Development of a gas chromatographymass spectrometry method for the determination of pesticides in gaseous and particulate phases in the atmosphere, Analytica. Chimica. Acta. 699, 57-65. crossref(new window)

2.
Breen, J.L., 2007. International trade implications of pesticide residues in food, Kor. J. Pesti. Sci. 58-64.

3.
Cooke, C.M., Shaw, G., Lester, J.N., Collins, C.D., 2004. Determination of solid-liquid partition coefficients (Kd) for diazinon, propetamphos and cis-permethrin, Science of The Total Environment 329(1-3), 197-213. crossref(new window)

4.
Fenoll, J., Hellin, P., Martinez, C.M., Miguel, M., Flores, P., 2007. Multiresidue method for analysis of pesticides in pepper and tomato by gas chromatography with nitrogen-phosphorus detection, Food Chem. 105(2), 711-719. crossref(new window)

5.
Jeon, Y.H., Kim, H.Y.. Hwang, J.I., Kim, J.H., Do, J.A., Im, M.H., Oh, J.H., Kwon, K.S., Lee, J.K., Lee, Y.D., Kim, J.E., 2011. Application of multiresidue analysis method of unregistered pesticides in Korea for imported food, Korean J. Environ. Agric. 30(3), 339-345. crossref(new window)

6.
Lee, E.M., Lee, H.R., Riu, M.J., Park, H.W., Na, Y.R., Song, H.H., Keum, Y.S., Zhu, Y., Kim, J.H., 2009. Establishment of analytical method of prochloraz in cabbage, apple, mandarin, pepper and hulled rice with GC-ECD, Korean J. Environ. Agri. 28(4), 427-434. crossref(new window)

7.
Lehotay, S.J., Kok, A., Hiemstra, M., Bodegraven, P., 2005. Validation of a fast and easy method for the determination of residues from 229 pesticides in fruits and vegetables using gas and liquid chromatography and mass spectrometric detection, J. AOAC Int. 88(2), 595-614.

8.
Pareja, L., Fernandez-Alba, A.R., Cesio, V., Heinzen, H., 2011. Analytical methods for pesticide residues in rice, Trends in Analytical Chemistry 30(2), 270-291. crossref(new window)

9.
Park, J.H., Kim, T.K., Oh, C.H., Kim, J.H., Lee, Y.D., Kim, J.E., 2004. Analysis of multiple pesticide residues in apples and pears using gas-liquid chromatography, Korean J. Environ. Agri. 23(3), 148-157. crossref(new window)

10.
Park, S.H., 2008. Safety management system of GM food, Food Sci. Indust. 41(2), 5-15.

11.
Qu, L.J., Zhang, H., Zhu, J.H., Yang, G.S., Aboul-Enein, H.Y., 2010. Rapid determination of organophosphorous pesticides in leeks by gas chromatography-triple quadrupole mass spectrometry, Food Chem. 122(1), 327-332. crossref(new window)

12.
Tarbah, F.A., Mahler, H., Temme, O., Daldrup, T,. 2001. An analytical method for the rapid screening of organophosphate pesticides in human biological samples and foodstuffs, Forensic Science International 121(1-2), 126-133. crossref(new window)

13.
Tolosa, I., Douy, B., Carvalho, F.P., 1999. Pesticide residue analysis in foodstuffs applying capillary gas chromatography with mass spectrometric detection, J. Chromatogr. A . 864(1), 121-136. crossref(new window)

14.
Tomlin, C.D.S., 2006. The Pesticide Manual (14th), BCPC, Hampshire, UK, pp. 232-233, 800-801, 870-871, 881-882, 1109, 1129.

15.
Yang, X., Zhang, H., Liu, Y., Wang, J., Zhang, Y.C., Dong, A.J., Zhao, H.T., Sun, C.H., Cui, J., 2011. Multiresidue method for determination of 88 pesticides in berry fruits using solid-phase extraction and gas chromatography-mass spectrometry: Determination of 88 pesticides in berries using SPE and GC-MS, Food Chem. 127(2), 855-865. crossref(new window)

16.
Zhao, Y.G., Shen, H.Y., Shi, J.W., Chen, X.H., Jin, M.C., 2011. Preparation and characterization of amino functionalized nano-composite material and its application for multi-residue analysis of pesticides in cabbage by gas chromatography-.triple quadrupole mass spectrometry, J. Chromatogr. A. 1218(33), 5568-5580. crossref(new window)