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Electrochemical synthesis of nanosized hydroxyapatite/graphene composite powder
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  • Journal title : Carbon letters
  • Volume 16, Issue 4,  2015, pp.233-240
  • Publisher : Korean Carbon Society
  • DOI : 10.5714/CL.2015.16.4.233
 Title & Authors
Electrochemical synthesis of nanosized hydroxyapatite/graphene composite powder
Vesna, Miskovic-Stankovic; Sanja, Erakovic; Ana, Jankovic; Maja, Vukasinovic-Sekulic; Miodrag, Mitric; Jung, Young Chan; Park, Soo Jin; Rhee, Kyong Yop;
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Electrochemical synthesis was employed to prepare a novel hydroxyapatite/graphene (HAP/Gr) composite powder suitable for medical applications as a hard tissue implant (scaffold). The synthesis was performed in a homogeneous dispersion containing Na2H2EDTA·2H2O, NaH2PO4 and CaCl2 with a Ca/EDTA/PO43− concentration ratio of 0.25/0.25/0.15M, along with 0.01 wt% added graphene nanosheets, at a current density of 137 mA cm−2 and pH value of 9.0. The field emission scanning electron microscopy and transmission electron microscopy observations of the composite HAP/Gr powder indicated that nanosized hydroxyapatite particles were uniformly placed in the graphene overlay. Raman spectroscopy, Fourier transform infrared spectroscopy and X-ray diffraction confirmed graphene incorporation in the HAP/Gr powder. The electrochemically prepared HAP/Gr composite powder exhibited slight antibacterial effect against the growth of the bacterial strain Staphylococcus aureus.
graphene;hydroxyapatite;electrochemical synthesis;composites;antibacterial activity;
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