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Preparation of Nanosized Gold Particles by Microwave Irradiation and Kinetics Study for Reduction of 4-Nitroaniline under Various Conditions
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  • Journal title : Elastomers and Composites
  • Volume 50, Issue 4,  2015, pp.274-278
  • Publisher : The Rubber Society of Korea
  • DOI : 10.7473/EC.2015.50.4.274
 Title & Authors
Preparation of Nanosized Gold Particles by Microwave Irradiation and Kinetics Study for Reduction of 4-Nitroaniline under Various Conditions
Kim, Jae Jin; Ko, Weon Bae;
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 Abstract
Nanosized gold particles were synthesized by microwave irradiation in a mixture composed of potassium tetrachloroaurate(III) n-hydrate, sodium citrate dihydrate and Tween 20. The synthesized gold particles were characterized by UV-vis spectrophotometer, scanning electron microscopy, and X-ray diffraction techniques. Using UV-vis spectroscopy, it was confirmed that gold nanoparticles act as a catalyst in the reduction of 4-nitroaniline with sodium borohydride to form 1,4-diaminobenzene. Additionally, we studied the kinetics of this reductive reaction in the presence of these gold nanoparticles under various conditions.
 Keywords
nanosized gold particles;4-nitroaniline;reductive reaction;catalytic activity;
 Language
English
 Cited by
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