JOURNAL BROWSE
Search
Advanced SearchSearch Tips
Preconcentration of Ultra Trace Amounts Bismuth in Water Samples Using Cloud Point Extraction with Na-DDTC and Determination by Electrothermal Atomic Absorption Spectrometry (ET-AAS)
facebook(new window)  Pirnt(new window) E-mail(new window) Excel Download
 Title & Authors
Preconcentration of Ultra Trace Amounts Bismuth in Water Samples Using Cloud Point Extraction with Na-DDTC and Determination by Electrothermal Atomic Absorption Spectrometry (ET-AAS)
Moghimi, Ali;
  PDF(new window)
 Abstract
.A new approach for a cloud point extraction-electrothermal atomic absorption spectrometric method was used for determining bismuth. The aqueous analyte was acidified with sulfuric acid (pH 3.0-3.5). Triton X-114 was added as a surfactant and natriumdiethyldithiocarbaminat (Na-DDTC) was used as a complexing agent. After phase separation at 50oC based on the cloud point separation of the mixture, the surfactant-rich phasen was diluted using tetrahydrofuran (THF). Twenty microliters (20 L) of the enriched solution and 10 l of 0.1% (w/v) Pd(NO3)2 as chemical modifier were dispersed into the graphite tube and the analyte determined by electrothermal atomic absorption spectrometry. After optimizing extraction conditions and instrumental parameters, a preconcentration factor of 195 was obtained for a sample of only 10 mL. The detection limit was 0.04 ng ml-1 and the analytical curve was linear for the concentration range of 0.04-0.70 ng mL-1. Relative standard deviations were <5%. The method was successfully applied for the extraction and determination of bismuth in water samples.
 Keywords
 Language
English
 Cited by
1.
Separation and preconcentration by a cloud point extraction procedure for determination of metals: an overview, Analytical and Bioanalytical Chemistry, 2009, 394, 3, 759  crossref(new windwow)
2.
A new voltammetric sensor based on thiol-functionalized polysiloxane film modified by lead nanoparticles for detection of Bi(III) ions, Electrochimica Acta, 2016, 208, 102  crossref(new windwow)
 References
1.
Bertholf, R. L.; Renoe, B. W. Anal. Chim. Acta 1982, 139, 287 crossref(new window)

2.
Burguera, M.; Burguera, J. L.; Rondon, C.; Garcia, M. I. J. Anal. At. Spectrom. 2001, 16, 1190 crossref(new window)

3.
Burguera, J. L.; Burguera, M.; Rivas, C.; Rondon, C.; Carrera, P.; Gallignani, M. Talanta 1999, 48, 885 crossref(new window)

4.
Thomas, D. W.; Hartley, T. F.; Coyle, P.; Sobecki, S. Handbook on Toxicity of Inorganic Compounds, Marcel Decker, New York, 1987, p. 15

5.
Thomas, D. W. Bismuth, in: E. Merian (Ed.), Metals and their Compounds in the Environment, VCH, Weinheim, 1991, p. 789

6.
Ribeiro, A. S.; Arruda, M. A. Z.; Cadore, S. Spectrochim. Acta B 2002, 57, 2113 crossref(new window)

7.
Acar, O.; Kllc, Z.; Rehber Turker, A. Anal. Chim. Acta 1999, 382, 329 crossref(new window)

8.
Rahman, L.; Corns, W. T.; Bryce, D. W.; Stockwell, P. B. Talanta 2000, 52, 833 crossref(new window)

9.
Morrow, A.; Witshire, G.; Huvsthous, A. At. Spectrosc. 1997, 18, 23

10.
Zhang, L.; Lu, Y.; Yang, G. Huaxue Fence 2000, 36, 26

11.
Feng, X.; Fu, B. Anal. Chim. Acta 1998, 371, 109 crossref(new window)

12.
Hinds, M. V.; Gregoie, D. C.; Ozaki, E. A. J. Anal. At. Spectrom. 1997, 12, 131 crossref(new window)

13.
Ostapczuk, P. Anal. Chim. Acta 1993, 273, 35 crossref(new window)

14.
Yang, H.-Y.; Chen, W.-Y.; Sun, I.-W. Talanta 1999, 50, 977 crossref(new window)

15.
Ye, R. D.; Khoo, S. B. Electroanalysis 1997, 9, 481 crossref(new window)

16.
Wang, C. M.; Sun, Q. Y.; Li, H. L. Electroanalysis 1997, 9, 645 crossref(new window)

17.
Ferri, T.; Paci, S.; Morabito, R. Anal. Dichim. 1996, 89, 245

18.
Hajian, R.; Shams, E. Anal. Chim. Acta 2003, 491, 63 crossref(new window)

19.
Alonso, A.; Almendral, M. J.; Baez, M. D.; Porras, M. J.; Lopez Lavln, C. Garcla de Marla, Anal. Chim. Acta 2000, 408, 129 crossref(new window)

20.
Sarkar, S. G.; Dhadke, P. M. Sep. Purif. Technol. 1999, 15, 131 crossref(new window)

21.
Lo, J. M.; Lin, Y. P.; Lin, K. S. Anal. Sci. 1991, 7, 455

22.
Tokman, N.; Akman, S.; Ozcan, M. Talanta 2003, 59, 201 crossref(new window)

23.
Yamini, Y.; Chaloosi, M.; Ebrahimzadeh, H. Talanta 2002, 56, 797 crossref(new window)

24.
Pournaghi-Azar, M. H.; Djozan, Dj.; Abdolmohammad zadeh, H. Anal. Chim. Acta 2001, 437, 217 crossref(new window)

25.
Moyano, S.; Gasquez, J. A.; Olsina, R.; Marchevsky, E. Martinez, L. D. J. Anal. At. Speltrom. 1999, 14, 259 crossref(new window)

26.
Silva, J. B. B.; Giacomelli, M. B. O.; Curtius, A. J. Analyst 1999, 124, 1249 crossref(new window)

27.
Moghimi, A. "Chinese Journal of Chemistry" 2007, 25, 640 crossref(new window)

28.
Kocjan, R.; Garbacka, M. Sep. Sci. Technol. 1994, 29, 799 crossref(new window)

29.
Manzoori, J. L.; Bavili-Tabrizi, A. Microchem. J. 2002, 72, 1 crossref(new window)

30.
Moghimi, A.; Tehrani, M. S.; Waqif Husain, S. Material Science Research India 2006, 3(1a), 27

31.
Garrido, M.; Di Nezio, M. S.; Lista, A. G.; Palomeque, M.; Fernández Band, B. S. Anal. Chim. Acta 2004, 502, 173 crossref(new window)

32.
Manzoori, J. L.; Karim-Nezhad, G. Anal. Sci. 2003, 19, 579 crossref(new window)

33.
Nascentes, C. C.; Arruda, M. A. Z. Talanta 2003, 61, 759 crossref(new window)

34.
Shemirani, F.; Baghdadi, M.; Ramezani, M.; Jamalim. R.; Analytica Chimica Acta 2005, 534, 163 crossref(new window)

35.
K. Evangelos, Paleologos, G. Athanasios, Vlessidis, I. Miltiadcs, Karayannis, P. Nicholaos, Evmiridis, Anal. Chim. Acta 2003, 477, 223 crossref(new window)

36.
Paleologos, E. K.; Giokas, D. L.; Tzouwara-Karayanni, S. M.; Karayannis, M. I. Anal. Chim. Acta 2002, 458, 241 crossref(new window)

37.
Manzoori, J. L.; Bavili-Tabrizi, A. Anal. Chim. Acta 2002, 470, 215 crossref(new window)

38.
Carasek, E.; Tonjes, J. W.; Scharf, M. Talanta 2002, 56, 185 crossref(new window)

39.
Chen, J.; Teo, K. C. Anal. Chim. Acta 2001, 450, 215 crossref(new window)

40.
J. Chen, K.C. Teo, Anal. Chim. Acta 2001, 434, 325 crossref(new window)

41.
Giokas, D. L.; Paleologos, E. K.; Tzouwara-Karayanni, S. M.; Karayannis, M. I. J. Anal. At. Spectrom. 2001, 16, 521 crossref(new window)

42.
Paleologos, E. K.; Stalikas, C. D.; Karayannis, M. I. Analyst 2001, 126, 389 crossref(new window)

43.
Kim, Y. S.; Choi, Y. S.; In, K. Bull. Korean Chem. Soc. 2001, 21, 137

44.
Luconi, M. O.; Fernanda Silva, M.; Olsina, R.A.; Fernandez, L. P.; Talanta 2000, 51, 123 crossref(new window)

45.
Mesquita da Silva, M. A.; Frescura, V. L. A.; Curtius, A. J. Spectrochim. Acta B 2000, 52, 803

46.
Ozturk, B. D.; Filik, H.; Tutem, E.; Apak, R. Talanta 2000, 53, 263 crossref(new window)

47.
Zaporozhets, O.; Petruniock, N.; Sukhan, V. Talanta 1999, 50, 865 crossref(new window)

48.
Concepcion Cerrato Oliveros, M.; de Blas, O. J.; Pavon, J. L. P.; Cordero, B. M. J. Anal. At. Spectrom. 1998, 13, 547 crossref(new window)

49.
Mesquita da Silva, M. A.; Azzolin Frescura, V. L.; Nome Aguilera, F. J.; Curtius, A. J. J. Anal. At. Spectrom. 1998, 13, 1369 crossref(new window)

50.
Manzoori, J. L.; Sorouradin, M. H.; Hajishabani, A. M. J. Anal. At. Spectrom. 1998, 13, 305 crossref(new window)

51.
Rjabuchin, S. Y.; Report IAEA/RL/50, Vienna, 1987

52.
He, B.; Ni, Z.-M. J. Anal. At. Spectorm. 1996, 11, 165 crossref(new window)

53.
Wei-Ming, Y.; Zhe-Ming, N. Spectrochim. Acta B 1997, 52, 241 crossref(new window)

54.
Acar, O.; Türker, A. R.; Kilic, Z., Fresenius, J. Anal. Chem. 1997, 357, 656 crossref(new window)

55.
Shan, X.-Q.; Wen, B. J. Anal. At. Spectrom. 1995, 10, 791 crossref(new window)

56.
Imai, S.; Hasegawe, N.; Nishiyama, Y.; Hayashi, Y.; Satio, K. J. Anal. At. Spectrom. 1996, 11, 601 crossref(new window)

57.
Havezov, I.; Detcheva, A.; Rendl, J. Mikrochim. Acta 1995, 119, 147 crossref(new window)

58.
Marczenko, Z. Separation and Spectrophotometric Determination of Elements, Ellis Horwood, Chichester, UK, 1986, p. 169