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Preparation, Characterization and Catalytic Activity of Tin Dioxide and Zero-Valent Tin Nanoparticles
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 Title & Authors
Preparation, Characterization and Catalytic Activity of Tin Dioxide and Zero-Valent Tin Nanoparticles
Pouretedal, H.R.; Shafeie, A.; Keshavarz, M.H.;
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 Abstract
The tin (IV) oxide nanoparticles are prepared by controlled precipitation method and calcined at temperatures of . The prepared nanoparticles characterized by XRD patterns, TEM image, IR and UV-Vis spectra. The XRD patterns and TEM image show the tetragonal structure and spherical morphology for nanoparticles, respectively. The photocatalytic activity of the prepared nanoparticles studied in degradation reaction of methylene blue (MB). The results show the size of nanoparticles, band-gap energy and photocatalytic activity of depends on the calcinations temperature. The nanoparticles calcined at indicated the highest photoreactivity. Also, the zero-valent tin (ZVT) nanoparticles with tetragonal structure are prepared by a reducing agent and used as a catalyst in degradation of MB. In basic pH of 11, the degradation >95% of MB at time 150 min obtained at presence of ZVT nanoparticles.
 Keywords
;Sn;Nanoparticles;Methylene blue;Photocatalyst;
 Language
English
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