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Development of Simultaneous Analysis for the Multi-residual Pesticides in the Ginseng Extract using Gas Chromatography
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 Title & Authors
Development of Simultaneous Analysis for the Multi-residual Pesticides in the Ginseng Extract using Gas Chromatography
Shin Yeong-Min; Lee Seon-Hwa; Son Yeong-Uk; Jeong Ji-Yoon; Jeoung Seoung-Wook; Park Heung-Jai; Kim Sung-Hun; Won Young-Jun; Lee Chang-Hee; Kim Woo-Seong; Hong Moo-Ki; Chae Kab-Ryong;
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 Abstract
The simultaneous analysis of multi-residual pesticides was developed using a gas chromatography (GC) method. In this study, a simple and reliable methodology was improved to detect 154 kinds of pesticides in sinseng extract sample by using a liquid-liquid extraction procedure, open column chromagraphy and chromatographic analysis by CC electron capture detector (ECD) and GC nitrogen-phosphorus detector (NPD). The 154 kinds of pesticides were classified in 4 groups according to the chemical structure. The extraction of pesticides was experimented with acetone and dichloromethane/petroleum ether in order, and cleaned up via open column chromatography packed with florisil . The final extract was concentrated in a rotator evaporator at until dryness. Then the residue was redissolved to 2ml with acetone, and analyzed by GC-ECD and GC-NPD. The applied concentration of pesticides was over . The recovery tests were ranged from to with standard deviations between 0.3 and of the standard spiked to the ginseng extract sample (Group ). The limit of detection (LOD) ranged from 0.001 to (Group ). The 9 kinds of pesticides were not detected. The developed method was applied satisfactory to the determination of the 154 kinds of pesticides in the ginseng extract with good reproducibility and accuracy.
 Keywords
Ginseng extract;Simultaneous analysis;Multi-residual pesticide;Gas chromatography;
 Language
Korean
 Cited by
1.
강원도 인삼재배지 농약 사용 실태,강혜순;박동식;황윤갑;김성문;

농약과학회지, 2007. vol.11. 3, pp.210-215
2.
숙지황 중 잔류농약과 중금속의 안전성 평가,김정호;양준영;문영수;

Journal of Environmental Science International, 2007. vol.16. 11, pp.1287-1293 crossref(new window)
3.
수삼과 홍삼농축액 중 유기인계와 유기염소계 농약의 잔류,김정호;

한국환경농학회지, 2007. vol.26. 4, pp.337-342 crossref(new window)
4.
경북북부 인삼 재배환경 중 중금속과 유기염소계 농약의 잔류,박수준;김정호;

Journal of Environmental Science International, 2010. vol.19. 10, pp.1203-1210 crossref(new window)
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