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Particle Size, Morphology and Color Characteristics of C.I. Pigment Red 57:1 : 1. Effect of Synthesis Conditions
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  • Journal title : Textile Coloration and Finishing
  • Volume 27, Issue 4,  2015, pp.229-244
  • Publisher : The Korean Society of Dyers and Finishers
  • DOI : 10.5764/TCF.2015.27.4.229
 Title & Authors
Particle Size, Morphology and Color Characteristics of C.I. Pigment Red 57:1 : 1. Effect of Synthesis Conditions
Seo, Hee Sung; Lee, Hyun Kyung; Yoo, Eui Sang;
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The effects of synthesis conditions on characteristics of the calcium-azo complex pigment, C.I. Pigment Red 57:1, were studied. It was mainly considered that the industrially required synthesis conditions for lowering electrical conductivity of the pigment solution keeping pigment quality such as particle size and color characteristics. Three parameters were chosen as control factors during the synthesis. The first was the amount of hydrochloric acid added to transform sodium nitrite into nitrous acid. The second was the amount of calcium chloride added to insolubilize the synthesized azo dye. The final factor was pH control during the coupling reaction. The electrical conductivity and pigment aggregate particle size were dependent on the amount of hydrochloric acid and calcium chloride. Higher HCl concentration gave brighter yellowish-red color because of smaller particle aggregate size and narrower size distribution. Amount of charged ions in the synthesis process might affect the "lake" formation resulting different particle aggregate size and color shade.
C.I. Pigment Red 57:1;synthesis conditions;electrical conductivity;particle size;color characteristics;
 Cited by
열전도성 입자를 활용한 시트용 점착제의 점착 특성과 방열특성 연구,김영수;박상하;최정우;공이성;윤관한;민병길;이승한;

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