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Optimization of Calcium Acetate Preparation from Littleneck Clam (Ruditapes philippinarum) Shell Powder and Its Properties
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 Title & Authors
Optimization of Calcium Acetate Preparation from Littleneck Clam (Ruditapes philippinarum) Shell Powder and Its Properties
Park, Sung Hwan; Jang, Soo Jeong; Lee, Hyun Ji; Lee, Gyoon-Woo; Lee, Jun Kyu; Kim, Yong Jung; Kim, Jin-Soo; Heu, Min Soo;
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 Abstract
The optimal condition for preparation of powdered calcium acetate (LCCA) which has high solubility, from calcined powder (LCCP) of the littleneck clam shell by response surface methodology (RSM) was examined. Increased molar ratio of LCCP led to reduced solubility, yield, color values, and overall quality. The critical values of multiple response optimization of independent variables were 2.57 M of acetic acid and 1.57 M of LCCP. The actual values (pH 7.0, 96.1% for solubility, and 220.9% for yield) under the optimized condition were similar to the predicted values. LCCA showed strong buffering capacity between pH 4.89 and 4.92 on addition of ~2 mL of 1 N HCl. The calcium content and solubility of LCCA were 21.9-23.0 g/100 g and 96.1-100.1%, respectively. The FT-IR and XRD patterns of LCCA were identified as calcium acetate monohydrate, and FESEM images revealed an irregular and rod-like microstructure.
 Keywords
littleneck clam;shellfish;calcined powder;calcium acetate;X-ray diffraction;
 Language
Korean
 Cited by
1.
개조개(Saxidomus purpuratus) 패각분말로부터 젖산칼슘의 제조 및 특성,윤인성;이균우;이현지;박성환;박선영;이수광;김진수;허민수;

한국수산과학회지, 2016. vol.49. 3, pp.301-309 crossref(new window)
2.
바지락(Ruditapes philippinarum) 패각 소성분말로 제조한 젖산칼슘의 특성,이균우;윤인성;이현지;이정석;김진수;허민수;

한국수산과학회지, 2016. vol.49. 4, pp.436-444 crossref(new window)
1.
Properties of Calcium Lactate Prepared from Calcined Littleneck Clam Ruditapes philippinarum Shell Powder, Korean Journal of Fisheries and Aquatic Sciences, 2016, 49, 4, 436  crossref(new windwow)
2.
Characterization of Calcium Lactate Prepared from Butter Clam Saxidomus purpuratus Shell Powder, Korean Journal of Fisheries and Aquatic Sciences, 2016, 49, 3, 301  crossref(new windwow)
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