X-Ray Fluorescence Analysis of $Ta_2O_5, Nb_2O_5, TiO_2, SnO_2$ and $Zr_O2$ in Tin-Slags

주석-슬랙 중 $Ta_2O_5, Nb_2O_5, TiO_2, SnO_2$, 및 $ZrO_2$의 X-선 형광분석

  • Young-Sang Kim (Department of Chemistry, Korea University) ;
  • Chong Wook Lee (Chemical Analysis Laboratory, Korea Advanced Institute of Science and Technology)
  • 김영상 (고려대학교 문리대학 화학과) ;
  • 이종욱 (한국과학기술연구원 화학분석실)
  • Published : 1983.08.20

Abstract

With the synthetic standards, valuable metals $(Ta_2O_5, Nb_2O_5, TiO_2, SnO_2$, and $ZrO_2$) in the tin slags have been determined by the x-ray fluorescence spectrometry. The powder sample and the standards are homogeneously mixed with anhydrous $Li_2B_4O_7$ and La_2O_3$ in weight ratio of 15 : 42 : 3 respectively. The mixed material is fused at $1,150^{\circ}C$ for 30 minutes to be changed into the glass bead. The bead is ground to (-) 325 mesh size and pelletized. The analytical results obtained in this work are consistent with the data obtained by other common methods within allowable error range. The standard deviation for $Ta_2O_5$ in PTS-H sample is 0.12 % at level of 3.40 % content.

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