Spectroscopic Studies on Crystallization of Na, TPA-ZSM-5 synthesized at Low Temperature and Atomospheric pressure

저온 상압에서 합성된 Na, TPA-ZSM-5의 결정화에 관한 분광학적 고찰

  • Yun, Young Ja (Department of Chemistry, Soongsil University) ;
  • Ha, Jae Mok (National Institute of Technology and Quality)
  • Received : 1996.09.19
  • Published : 1997.02.25


Na, TPA-ZSM-5 with Si / Al mole ratio of about 130 was synthesized at low temperature and atmospheric pressure. These intermediate products were characterized by using XRD, XRF, FT-IR, NMR, and SEM. As a result, intermediate product were different from those that synthesized by autoclave method but spectroscopic characteristics of the final products showed to be in the typical ZSM-5 region. The defect sites were observed in the final product and removed by calcination at $540^{\circ}C$. Na, TPA-ZSM-5, aboveall, was synthesized at this condition within 48hr.