Quantitative Analysis of trans-Resveratrol in Red Wines by Solid Phase Extraction and LC/MS

고체상 추출법과 LC/MS를 이용한 적포도주 중의 trans-Resveratrol 분석

  • Park, Gyo-Beom (Chemical Analysis Laboratory, Korea Research Institute of Chemical Technology) ;
  • Moon, Hyoung-Sil (Chemical Analysis Laboratory, Korea Research Institute of Chemical Technology) ;
  • Lee, Sueg-Geun (Chemical Analysis Laboratory, Korea Research Institute of Chemical Technology)
  • Received : 2003.02.17
  • Accepted : 2003.03.18
  • Published : 2003.04.25

Abstract

In order to determine the contents of trans-resveratrol in red wine, which was mainly consumed in Korea, both LC/MS-ESI and LC/MS-APCI methods were used after solid-phase (Sep-Pak $C_{18}$-cartridges) extraction. The contents of trans-resveratrol obtained by LC/MS-ESI were detected in the range of $0.06-4.31{\mu}g/mL$. The recoveries were ranged from 88.4 to 97.9%. The values of relative standard deviation were ranged from 0.6 to 4.6% and the detection limit was $0.001{\mu}g/mL$. The contents of trans-resveratrol obtained by LC/MS-APCI were detected in the range of $0.09-4.02{\mu}g/mL$ and the detection limit was $0.005{\mu}g/mL$.

Keywords

trans-resveratrol;wine;LC/MS;LC/MS-APCI

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