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Size-controlled Growth of Fe Nanoparticles in Gas Flow Sputtering Process

  • Sakuma, H. (Department of Electrical and Electronic Engineering, Utsunomiya University) ;
  • Aoshima, H. (Department of Electrical and Electronic Engineering, Utsunomiya University) ;
  • Ishii, K. (Department of Electrical and Electronic Engineering, Utsunomiya University)
  • Published : 2006.09.01

Abstract

In grain oriented electrical steel process, hot band annealing has thought to be essential for obtaining good magnetic properties. New hot rolling method of heavy reduction in early hot rolling stage was applied to obtain good magnetic properties in GO process without hot band annealing. Hot rolling was carried out by varyinghot rolling reduction distribution along hot rolling pass. The heavy hot rolling reduction in rear stand improves the magnetic flux density in the case of no hot band annealing. The hot band specimens of the heavy reduction in front stand shows the elongated hot deformed microstructures in the center layer and strong {001}<110> texture.On the contrary, the heavily reduced specimens in rear stand shows the recrystallization in the center layer of hot band and strong {111}<112> and {110}<001> textures.

References

  1. X. X. Zhang, B. X. Qin, G. H. Wen, Y. S. and Kwok, K. K. Fung, Mater. Sci. Eng. C 16, 119 (2001) https://doi.org/10.1016/S0928-4931(01)00285-5
  2. Y. Li, P. Xiong, S. von Molnar, S. Wirth, Y. Ohno, and H. Ohno, Appl. Phys. Lett. 80, 4644 (2002) https://doi.org/10.1063/1.1487921
  3. W. Z. Li, S. S. Xie, L. X. Qian, B. H. Chang, B. S. Zou, W. Y. Zhou, R. A. Zhao, and G. Wang, Science 274, 1701 (1996) https://doi.org/10.1126/science.274.5293.1701
  4. B. Giesen, H. R. Orthner, A. Kowalik, and P. Roth, Chem. Eng. Sci. 59, 2201 (2004) https://doi.org/10.1016/j.ces.2004.02.013
  5. A. Tasaki, S. Tomiyama, S. Iida, N. Wada, and R. Uyeda, Jpn. J. Appl. Phys. 4(10), 707 (1965) https://doi.org/10.1143/JJAP.4.707
  6. D. Farrell, S. A. Majetich, and J. P. Wilcoxon, J. Phys. Chem. B 107(40), 11022 (2003) https://doi.org/10.1021/jp0351831
  7. K. Ishii, K. Amano, and H. Hamakake, J. Vac. Sci. Technol. A 17(1), 310 (1999) https://doi.org/10.1116/1.581585
  8. K. Ohta, Basis of Magnetics II, Kyoritsu, Tokyo (1973), pp. 336 (in Japanese)
  9. S. Muto, Handbook of Statistical Analysis, Asakura, Tokyo (1995), pp. 131 (in Japanese)
  10. A. Slawska-Waniewska, A. Roig, M. Gich, Ll. Casas, K. Racka, N. Nedelko, and E. Molins, Phys. Rev. B 70, 054412 (2004) https://doi.org/10.1103/PhysRevB.70.054412
  11. K. Takahashi, Basis of Aerosol Dynamics, Morikita, Tokyo (2003), chap. 6 (in Japanese)

Cited by

  1. Preparation and Characterization of Fe–N Nanoparticles by Gas Flow Sputtering vol.47, pp.1, 2008, https://doi.org/10.1143/JJAP.47.780