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Analytical method of New POPs in environmental samples

환경 중 신규 POPs 분석방법 고찰

  • Shin, Sun-Kyoung (National Institute of Environmental Research of Environmental Research) ;
  • Park, Jin-Soo (National Institute of Environmental Research of Environmental Research) ;
  • Kang, Young-Yeul (National Institute of Environmental Research of Environmental Research) ;
  • Lee, Su-Young (National Institute of Environmental Research of Environmental Research) ;
  • Chun, Jin-Won (National Institute of Environmental Research of Environmental Research) ;
  • Kim, Dong-Hoon (National Institute of Environmental Research of Environmental Research) ;
  • Yeon, Jin-Mo (National Institute of Environmental Research of Environmental Research)
  • 신선경 (국립환경과학원 환경건강위해성연구부 화학물질거동연구과) ;
  • 박진수 (국립환경과학원 환경건강위해성연구부 화학물질거동연구과) ;
  • 강영렬 (국립환경과학원 환경건강위해성연구부 화학물질거동연구과) ;
  • 이수영 (국립환경과학원 환경건강위해성연구부 화학물질거동연구과) ;
  • 전진원 (국립환경과학원 환경건강위해성연구부 화학물질거동연구과) ;
  • 김동훈 (국립환경과학원 환경건강위해성연구부 화학물질거동연구과) ;
  • 연진모 (국립환경과학원 환경건강위해성연구부 화학물질거동연구과)
  • Received : 2010.02.22
  • Accepted : 2010.03.16
  • Published : 2010.04.25

Abstract

The purpose of this study is to set up the analytical method of new persistent organic pollutants (POPs) such as chlordecone, endosulfan, ${\alpha}$-HCH, ${\beta}$-HCH, ${\gamma}$-HCH. The analytical methods for these compounds listed as new POPs by the Stockholm Convention need to be newly established. Therefore, we proposed the analytical method for 5 organic chlorinated pesticides (OCPs) and then applied the analytical method to environmental samples. To do this, the pre-treatment such as florisil and activated carbon cleanup process in the Korean official method for classic POPs had been reviewed. All of compounds except chlordecone were pre-treated simultaneously with reviewed cleanup process and detected by GC/MS and HRGC/HRMS respectively. There is a problem that chlordecone could not get a high sensitivity by GC analysis, but in this study GC/MS method was proposed.

Keywords

New POPs;HCH;endosulfan;chlordecone;GC/MS;HRGC/HRMS

References

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Cited by

  1. Development of Multi-residue Analysis and Monitoring of Persistent Organic Pollutants (POPs) - Used Organochlorine Pesticides in Korea vol.20, pp.4, 2016, https://doi.org/10.7585/kjps.2016.20.4.319
  2. Persistent Organic Pollutants (POPs) Residues in Greenhouse Soil and Strawberry Organochlorine Pesticides vol.35, pp.1, 2016, https://doi.org/10.5338/KJEA.2016.35.1.05