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Determination of polycyclic aromatic hydrocarbons in processed foods

가공식품 중 다환방향족탄화수소 분석

  • Hu, Soo-Jung (Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation) ;
  • Jin, Sun-Hee (Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation) ;
  • Lee, Kwang-Ho (Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation) ;
  • Choi, Dong-Mi (Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation)
  • 허수정 (식품의약품안전평가원 식품위해평가부) ;
  • 진선희 (식품의약품안전평가원 식품위해평가부) ;
  • 이광호 (식품의약품안전평가원 식품위해평가부) ;
  • 최동미 (식품의약품안전평가원 식품위해평가부)
  • Received : 2010.01.07
  • Accepted : 2010.03.02
  • Published : 2010.04.25

Abstract

In this study, the following concentrations of some PAHs (Polycyclic Aromatic Hydrocarbons) were investigated; [benzo(a)anthracene, chrysene, benzo(b)fluoranthene, benzo(k)fluoranthene, benzo(a)pyrene, dibenzo(a,h)anthracene, benzo(g,h,i)perylene, indeno(1,2,3-c,d)pyrene] in processed foods (n=165) and cooked meats (n=45) and established the analytical method by characteristics of processed foods. The methodology involved extraction (alkali digestion, liquid-liquid extraction, microwave extraction), clean-up on Sep-Pak Florisil Cartridges and determination by HPLC/FLD (High Performance Liquid Chromatography/Fluorescence Detector). The recovery of overall method for 8 PAHs spiked into these products ranged from 92 to 103%. The mean level of detected foods was found to be benzo(b)fluoranthene $0.9\;{\mu}g/kg$ in smoked salmon, benzo(b)fluoranthene $1.0\;{\mu}g/kg$, benzo(k)fluoranthene $0.3\;{\mu}g/kg$, benzo(a)pyrene $0.9\;{\mu}g/kg$ in dried banana, benzo(b)fluoranthene $0.2\;{\mu}g/kg$, benzo(k)fluoranthene $0.1\;{\mu}g/kg$, benzo(a)pyrene $0.2\;{\mu}g/kg$ in smoked chicken, benzo(b)fluoranthene $1.3\;{\mu}g/kg$, benzo(k)fluoranthene $0.3\;{\mu}g/kg$, benzo(a)pyrene $0.9\;{\mu}g/kg$ in charcoal grilled pork, respectively.

Keywords

Polycyclic aromatic hydrocarbons;benzo(a)pyrene;processed food;HPLC/FLD

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Cited by

  1. Study on analysis of PAHs in consumer products vol.27, pp.4, 2014, https://doi.org/10.5806/AST.2014.27.4.201
  2. Analysis of benzo[a]pyrene content from smoked food products in Korea vol.21, pp.4, 2012, https://doi.org/10.1007/s10068-012-0142-x
  3. Analysis of Benzo[a]pyrene Content and Risk Assessment vol.31, pp.6, 2011, https://doi.org/10.5851/kosfa.2011.31.6.960