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Determination of phenol using solid-phase extraction and HPLC/MSD/FLD in water

고체상추출법과 HPLC/MSD/FLD를 이용한 수질중의 페놀 분석

  • 이태준 (강원도보건환경연구원) ;
  • 박근영 (강원도보건환경연구원) ;
  • 표동진 (강원대학교 자연과학대학 화학과)
  • Received : 2015.08.11
  • Accepted : 2015.10.27
  • Published : 2015.12.25

Abstract

An analytical method for determining phenol considered priority pollutants of the US EPA and precursor of toxic phenolic compounds by solid-phase extraction (SPE) and high performance liquid chromatographic systems (HPLC) equipped with fluorescence and mass selective detectors have been developed. The SPE process for sample preconcentration was performed on a commercially available Oasis HLB cartridge packed with polymeric sorbents. The effect of pH, elution solvent, and elution volume on the recoveries of the analytes were investigated with HPLC/FLD. Average recovery of >87.0% was achieved with 60 mg sorbents using 5 mL of methanol as an elution solvent at pH=3.

Keywords

phenol;hplc;solid phase extraction(spe);hplc/msd

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