Synthesis of Multi-walled Carbon Nanotubes and Nanofibers on a Catalytic Metal Substrate Using an Ethylene Inverse Diffusion Flame as a Heat Source

에틸렌 역확산화염을 열원으로 사용하여 촉매금속 기판 상에 합성한 탄소나노튜브와 탄소나노섬유

  • 이교우 (한국과학기술연구원(KIST) 대기자원연구센터) ;
  • 정종수 (한국과학기술연구원(KIST) 대기자원연구센터) ;
  • 강경태 (생산기술연구원 생산시스템본부 청정설계기술팀) ;
  • 황정호 (연세대학교 기계공학과)
  • Published : 2004.04.28

Abstract

Synthesis of carbon nanotubes and nanofibers on a catalytic metal substrate, using an ethylene fueled inverse diffusion flame, was investigated. Multi-walled carbon nanotubes, with diameters of 20 - 60nm, were formed on the substrate coated with nickel-nitrate in the region of 5 - 6mm from the flame center along the radial direction. The gas temperature for this region was ranging from about 1400 to 900K. Nickel particles originated from the coated nickel-nitrate on the substrate were the major catalyst for the formation of the nanomaterials. HR-TEM and Raman spectrum revealed that synthesized carbon nanotubes had multi-walled structures with some defective graphite layers at walls.

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