Formation of Shell-Shaped Carbon Nanoparticles through Critical Transition in Irradiated Acetylene

레이저가 조사된 아세틸렌에서의 임계전이를 거쳐서 형성된 쉘 형상 카본 나노입자에 관한 연구

  • 최만수 (서울대학교 기계항공공학부 나노입자제어기술연구단) ;
  • ;
  • 김영정 (서울대학교 기계항공공학부 나노입자제어기술연구단) ;
  • ;
  • 이상훈 (서울대학교 기계항공공학부 나노입자제어기술연구단)
  • Published : 2004.11.03

Abstract

Shell shaped hollow carbon nanoparticles are synthesized in the oxygen-hydrogen diffusion flame with $C_{2}H_{2}$ as precursor when it is irradiated with $CO_{2}$ laser of certain power. Below this power of laser, we couldn't get any other but amorphous soot. This shell shaped hollow carbon nanoparticles shows outer wall of high degree of crystallinity with void space inside of itself. And size distribution of these nanoparticles is measured with TEM image analysis. Also the structural comparison between this carbon nanoparticle and soot is done by Raman and XRD measurement. These results show this carbon nanoparticles are of grapheme structure, which means it has good crystallinity when compared with soot.

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