Effect of $Al_2O_3$ on Hot-Press of ${\alpha}-SiC$ and Mechanical Properties

알루미나의 첨가가 ${\alpha}-SiC$의 가압소결 및 기계적 성질에 미치는 영향

  • 이수영 (한국기계연구소 요업재료실) ;
  • 고재웅 (한국기계연구소 요업재료실) ;
  • 김해두 (한국기계연구소 요업재료실)
  • Published : 1991.07.01

Abstract

Submicron ${\alpha}-SiC$ powder with $Al_2O_3$ addition was hot-pressed under the controlled heating and pressurizing schedule. $SiO_2$ layer on ${\alpha}-SiC$ powder was effective for the sintering of ${\alpha}-SiC$ powder when $Al_2O_3$ was used as an additive. Applying of pressure under the controlled schedule accelerated the rearrangment of SiC grains, yielding 98% of theoretical density of SiC even at $1900^{\circ}C$. Flexural strength of the specimen containing 2 wt% $Al_2O_3$ was increased as increasing the hot-pressing temperature up to $2050^{\circ}C$ and maximum value was 800 MPa, while the flexural strength of the specimen containing 10 wt% $Al_2O_3$ was decreased as increasing the hot-pressing temperature above $2000^{\circ}C$ due to the formation of continuous grain boundary phase. Fracture toughness of the specimens was in the range of $3.5~4.5\;MNm^{-3/2}$ regardless of the amount of $Al_2O_3$ addition.

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References

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