Bauxite로부터 습식 산처리법에 의한 알루미나 분체의 제조 및 그 이용에 관한 연구(III) : Aluminum Hydrate Gel의 분산에 의한 알루미나 분체의 소결성 향상

A Study on the Preparation of Alumina Powders from Bauxite by Wet Acid Process and Their Utilization (III) : Effects of the Dispersion of Aluminum Hydrate Gel on the Sintering Behavior of Alumina Powder

  • 조철구 (경상대학교 무기재료공학과) ;
  • 정원도 (경상대학교 무기재료공학과) ;
  • 배원태 (경상대학교 무기재료공학과)
  • 발행 : 1993.04.01

초록

Dispersant was used to avoid the agglomeration of aluminum hydrate precipitate and improve the sinterability of calcined alumina powder. The mean particle size of the aluminum hydrate precipitates was 0.26${\mu}{\textrm}{m}$ and 0.44${\mu}{\textrm}{m}$ when ball-milled with and without dispersant, respectively. After calcination at 110$0^{\circ}C$ for 5 hours, the size of the alumina powder without dispersant increased to 0.84${\mu}{\textrm}{m}$, while with dispersant slightly decreased to 0.22${\mu}{\textrm}{m}$. The most thermally active alumina powder was obtained from the sample calcined at 110$0^{\circ}C$ for 5 hours with the 1% dispersant concentration. Using the calcined alumina powder at the above optimized condition, the specimen showed fired density of 3.94g/㎤, 4-point MOR of 364MPa, and KIC of 3.26MPam1/2 after sintered at 155$0^{\circ}C$ for 3 hours.

키워드

참고문헌

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