Synthesis and properties of $Al_2O_3-SiC$ Composites from Alkoxides III. Effect of Composite Powder Type on the Sintering Characteristics and Properties of $Al_2O_3-SiC$ Comopsites

알콕사이드로부터 $Al_2O_3-SiC$ 복합재료의 제조 및 특성 III. 복합분말의 형태에 따른 $Al_2O_3-SiC$ 복합재료의 소결 특성 및 물성

  • 이홍림 (연세대학교 공과대학 세라믹공학과) ;
  • 김규영 (연세대학교 공과대학 세라믹공학과)
  • Published : 1993.04.01

Abstract

Three types of dispersed, coated and mechanically mixed SiC reinforced Al2O3 composite powders were used to investigate the effect of composite powder type on sintering characteristics and properties of Al2O3-SiC composites. Sinterability of coated type composite powders was superior to that of other composite powders when they were pressureless sintered at 1500~1$700^{\circ}C$ for 2h in Ar atmosphere. However, sinterabilities (>98% TD) of each type of composite powders were similar when they were hot pressed at 180$0^{\circ}C$ for 1h under 30MPa in N2 atmosphere. SiC powders were randomly distributed in the specimen prepared from dispersed type composite powders, whereas homogeneously distributed for coated type specimens. It was found that SiC powders inhibited the grain growth of Al2O3, and fracture toughness was increased by the increment of crack growth resistance due to residual stress by secondary SiC particles within Al2O3 grains.

Keywords

References

  1. J. Am Ceram. Soc. v.55 no.5 Strength Degradation and Crack Propagation on Thermally Shocked Alumina T.G Gupta
  2. Yogyo-Kyokai-Shi v.94 no.8 Microstructure and Mechanical Properties of $Al_2O_3-SiC$ Composites A. Nakahira;K. Niihara;T. Hirai
  3. J. of Japan Society of Powd & Powd Metal. v.37 no.7 Studies on the Development of $Al_2O_3-SiC$ Ceramics Y. Katsumura;K. Kobori;H Suzuki
  4. J. Am. Ceram. Soc. v.72 no.8 Pressureless Sintering of Alumina-Titanium Carbide Composites Y.W. Kim;J.G. Lee
  5. Am. Ceram. Soc. Bull. v.66 no.2 Sintered $Al_2O_3-SiC$ Whisker Composites T.N Tiegs;P.E. Becher
  6. J. Am. Ceram. Soc. v.67 no.12 Toughening Behavior in SiC Whisker Reinforced Alumina P.F. Becher;G.C. Wei
  7. CERAMICS: TOWARD THE 21st CENTURY: Centennial International Symposium Structural Ceramic Nanocomposites by Sintering Method. Roles of Nanosize Particle K. Niihara;A. Nakahira;Soga, A. Kato(ed.)
  8. セラミクス. v.27 no.4 ナノ微構造と破壞 新原晧一
  9. Ultrastructure Processing of Ceramics, Glasses and Composites Potential Impact of Ultrastructural Processing on Government and Industry D.R. Ulrich;L.L. Hench(ed.)
  10. J. Kor. Ceram Soc. Synthesis of $Al_2O_3-SiC$ Composites from Alkoxides and Their Characterization. I. Synthesis of Dispersed Type$Al_2O_3-SiC$ Composite Powders H.L. Lee;K.Y. Kim
  11. J. Kor. Ceram. Soc. Synthesis of $Al_2O_3-SiC$ Composites from Alkoxides and Their Characterization.II Synthesis of Coated Type $Al_2O_3-SiC$ Composite Powders H.L. Lee;K.Y. Kim
  12. Ceram. Sci Eng Proc. Lee;Brun
  13. 窯業基礎討論會講演要旨集 v.59 no.21 新原晧一
  14. J. Am. Ceram. Soc. v.73 no.7 Pressureless Sintering of SiC Whisker Reinforced $Al_2O_3$ Composites: I. Effect of Matrix Powder Surface Area H.W. Lee;M.D. Sacks
  15. J. Am. Ceram. Soc v.73 no.7 Pressureless Sintering of SiC Whisker Reinforced$Al_2O_3$ Composites: II. Effect of Sintering Additives and Green Body Infiltration HW. Lee;M.D. Sacks
  16. Ceramic Powder Science Ⅱ, B. Effects of Foreign Oxides on Grain Growth and Densification of Sintered $Al_2O_3$ S. Sumita;H.K. Bowen;G.L. Messing(ed.)
  17. Euro Ceramics v.1 Effect of SiO₂on Grain Growth and Densification of Alumina Prepared by Sol-Gel Technique H.D. Kim;H.K. Kang;G.de(ed.);R.A. Terpstra(ed.);R. Metselaar(ed.)
  18. J. Am. Ceram. Soc v.75 no.8 Factors Controlling the Sintering of Ceramic Particulate Composites: Ⅱ. Coated Inclusion Particles C.L. Hu;M.N. Rahaman
  19. J. of Jpn Soc. of Powd and Powd Metal. v.35 no.6 Improvement of Sinterbility of $Al_2O_3-SiC$ Ceramics Y. Katsumura;M. Kobayashi