Sintering Behavior of Ultra-fine Hydroxyapatite Powders Synthesized by Hydrothermal Reaction

수열반응으로 합성한 Hydroxyapatite 초미분말의 소결특성

  • 최재웅 (한양대학교 무기재료공학과) ;
  • 조성원 (한양대학교 무기재료공학과) ;
  • 최상홀 (한양대학교 무기재료공학과)
  • Published : 1994.11.01

Abstract

Ultra-fine hydroxyapatite powder were synthesized by the hydrothermal reaction at 10 atm, 3 hrs of Ca(OH)2 suspension with (NH4)2HPO4 solution, and were characterized sintering behavior. Sintered bodies of hydroxyapatite powders which synthesized by hydrothermal reaction method has less weight loss, less sintering shrinkage and superior mechanical property, and was more dense than sintered bodies of hydroxyapatite powder which synthesized by wet method. Sintered bodies were hydroxyapatite single phase. When soack in Ringer's solution for 2 weeks, hydroxyapatite powders preserved hydroxyapatite and sintered body absorbed trace of Ca2+ ion with soaked time.

Keywords

References

  1. J. Chem. Soc. no.9 Hydrothermal Synthesis of Ultrafine hydroxyapatite Single Crystal K. Ioku;M. Yoshimura;S. Somiya
  2. 한국요업학회지 v.29 no.12 수열반응에 의한 hydroxyapatite 초미분말의 제조 민경소;최재웅;최상흘
  3. Am. Ceram. Soc. Bull. v.66 no.9 Hydrothermal Processing of Ceramics S.I. Hirano
  4. Am. Ceram. Soc. Bull. v.67 no.10 Hydrothermal Synthesis of Advanced Ceramics Powders W.J. Dawson
  5. J. Am. Ceram. Soc. v.74 no.4 Rapid and Continuous Hydrothermal Crystallization of Metal Oxide Particles in Supercritical Water T. Adshiri;K. Kanazawa;K. Arae
  6. Am. Ceram. Soc. Bull. v.68 no.5 International Trends in Powder Technology L.M. Shepparo
  7. J. Am. Ceram. Soc. v.73 no.6 Hydrothermal Preparation of Calcium hydroxyapatite Powders T. Hattori;Y. Iwadate
  8. J. Mat. Sci. v.10 no.2016 Equilibrium Penny-like Cracks in Indentation Fracture B.R. Lawn;E.R. Kuller
  9. J. Cer. Soc. Japan v.95 no.8 Bonding between bioactive Glasses Glasses-Ceramics or Ceramics in a Simulated Body Fluid T. KoKubo;T. Hayashi;S. Sakka;T. Kitsugi;T. Yamamuro
  10. Proceeding of the First Korea-Japan Seminar on New Ceramics Bioceramics-Apatite Bioceramics H. Monma
  11. Kagakuno Ryoiki v.27 no.9 Recent Progress the Chemistry of Calcium Phosphates, Especially Apatite-Their Composition, Structure and Properties T. kanazawa;H. Monma
  12. D. N. Misraed. Adsorption and Surface Chemistry of hydroxyapatite S. Chacer;D.W. Feurstenau