Preparation and Characterization of $TiO_2$ Membranes for Microfiltration

$TiO_2$ 정밀여과막의 제조 및 특성

  • 한상욱 (연세대학교 세라믹공학과) ;
  • 최세영 (연세대학교 세라믹공학과) ;
  • 현상훈 (연세대학교 세라믹공학과) ;
  • 조철구 (유동기업 (주) 부설연구소) ;
  • 강한규 (유동기업 (주)부설연구소)
  • Published : 1996.06.01

Abstract

TiO2 membranes for microfiltration were prepared on $\alpha$-alumina support tube by slurry coating. The coating layer was obtained by flowing TiO2 slip on the inner surface of the alumina support. TiO2 membranes were heat-treated at 9$25^{\circ}C$ for 2 hrs. The thickness of the unsupported membrane was about 10${\mu}{\textrm}{m}$. The mean pore diameter of the membranes were 0.09 and 0.15${\mu}{\textrm}{m}$ respectively and the pure water flux was 900~1,200ι/m2.hr at room temperature and 1 bar. For a possible application of oily wastewater treatement an kerosene/wa-ter emulsion was separated in terms of flux and removal efficiency. In 60 min of operating time the flux of TiO2 membranes was 50~100 ι/m2.hr and removal efficiency was over 97% at 3kgf/cm2 of operating pres-sure and 600 ml/min of flow rate. TiO2 membranes could be recycled by reheat treatments at $600^{\circ}C$ for 2 hrs.

Keywords

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