Journal of the Korean Ceramic Society (한국세라믹학회지)

The Korean Ceramic Society (한국세라믹학회)
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Fabrication of 3Y-TZP/SUS316 Functionally Graded Material by Slip Casting Method Using Alumina Mold

알루미나몰드를 사용한 슬립캐스팅법에 의한 3Y-TZP/SUS316계 경사기능재료의 제조

  • 여정구 (한양대학교 공과대학 무기재료공학과) ;
  • 정연길 (한양대학교 공과대학 무기재료공학과) ;
  • 이세훈 (한양대학교 공과대학 무기재료공학과) ;
  • 최성철 (한양대학교 공과대학 무기재료공학과)
  • Published : 1997.01.01
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Abstract

3Y-TZP/SUS316 Functionally Graded Material (FGM) was fabricated by slip casting method. Alumina mold was used to overcome problems of gypsum mold in slip casting process, and the optimal dispersion con-ditions of 3Y-TZP/SUS316 binary slurries was determined using electrokinetic sonic amplitude and a viscometer, and observing sedimentation behavior. The properties of the specimens casted by gypsum mold and alumina mold were compared in terms of changes in shrinkage rate, drying and sintering conditions, and microstructure. It was found that the specimens obtaine from the alumina mold showed a clean surface, easier thickness control of each layer, and higher productivity. Especially, no degradation was observed in the SUS316 prepared using alumina mold. Thus it is desirable to use porous alumina mold rather than gyp-sum mold for the slip casting of 3Y-TZP/SUS316-FGM.

3Y TZP/SUS316계 경사기능재료를 슬립캐스팅법을 이용하여 제조하였다. 슬립캐스팅 공정에서 석고몰드를 대체하기 위해 알루미나몰드를 제조하였고, 3Y-TZP/SUS316 2상 슬러리의 최적 분산조건을 ESA, 점도계, 침전거동의 관찰 등을 통해 결정하였으며, 석고몰드와 알루미나몰드로 캐스팅한 시험편의 제반 특성을 소결수축율변화, 건조 및 소결거동, 미세구조 관찰 등으로 조사하였다. 그 결과 알루미나몰드를 사용하여 제조된 시험편에서는 석고몰드 사용시 나타나는 표면에서의 오염이 관찰되지 않았으며, 각 층의 두께조절이 쉬웠고 높은 재현성을 나타냄을 알 수 있었다. 특히 알루미나몰드를 사용하여 제조한 SUS316에서는 어떤 열화현상도 관찰되지 않았다. 결국 슬립캐스팅 공정으로 3Y-TZP/SUS316계 경사기능재료를 제조함에 있어서 기존의 석고몰드보다 다공질 알루미나몰드의 사용이 바람직하다는 것을 알 수 있었다.

Keywords

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