Preparation of Indium Oxide Particles by Spary Pyrolysis of Indium Nitrate

질산 인듐 수용액의 초음파 분무열분해에 의한 산회인듐 입자의 제조

  • 김기영 (삼성전관 기초연구 LAB) ;
  • 박승민 (한국과학기술원 화학공학과)
  • Published : 1998.06.01

Abstract

Agglomeration-free indium oxide particles were produced by ultrasonic pyrolysis of indium nitrate(3 hy-drate) solution. Th mean size of particles was increased from 3 $\mu\textrm{m}$ to 11$\mu\textrm{m}$ with increasing intial con-centrations of indium nitrate from 0.05mol% to 4.83 mol% When the input rate of indium nitrate solution was increased from 0.1 cm3/min to 0.8cm3/min the size of particles remained same and only the pro-duction rate of particles was increased. At 300$^{\circ}C$ the particles were white color with low crystallinity. But the color turned into yellow with increasing reaction temperature. The change of particle size was not ob-served with increasing temperatuer up to 700$^{\circ}C$ IR spectrum and TGA analysis confirmed that the purity of indium oxide was increased with temperature of reaction.

Keywords

References

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