Properties of Chopi Oleoresin Extracted with Various Solvents and Effects of Extraction Conditions on Volatile Components

초피 Oleoresin 제조시 용매에 따른 추출물특성과 추출조건에 따른 휘발성 성분 변화

  • 최용희 (경북대학교 식품공학과) ;
  • 허상선 (경북대학교 농업과학기술연구소) ;
  • 배동호 (건국대학교 응용생물화학과) ;
  • 김상욱 (경북대학교 식품공학과)
  • Published : 1998.06.01

Abstract

Such extraction conditions as the kinds of solvent, extracting temperature, extracting time, ratio of material to solvent and particle size of material, were studied to maximize the extraction of oleoresin from chipi. Larger amount of soluble solids were extracted from seeds with nonpolar solvents (hexane, pentane, ether) for extraction, because the seeds contained large amount of crude fats and monoterpene(limonene) volatile compounds. Larger amount of soluble solids were extracted from peel with polar solvents(methanol, ethanol) of extraction because of large amount of water soluble colors, sugars and oxygenated terpene bolatile compounds in the peel. The application of the solvents in intermediate polarity (dichloromethane, acetone) resulted in more effective extraction of soluble solid and volatile compounds. Expecially, dichloromethane was an excellent solvent in extraction of volatile compounds. In the concern of volatile compound recovery yield, the optimum extraction conditions, such as temperature, time, mixing ratio of material to dichloromethane and mean particle size, were $25^{\circ}C$, 10min, 1:10(w/v), 355~250${\mu}{\textrm}{m}$ for chopi peels and 3$0^{\circ}C$, 10min, 1:8(w/v), 355~250${\mu}{\textrm}{m}$ for chopi seeds, respectively.

Keywords

References

  1. 식물학 대사전 송규택
  2. 식품가공저장학 유태종
  3. 식품재료학 문범수;이갑상
  4. スパイス百科事典 武政三男
  5. 新編日本食品事典 杉田浩一;堤忠一;森雅中編
  6. 한국음식 역사와 조리 윤서석
  7. 고려이전의 식생활사 이성우
  8. Microbiology, Technology Spices and condiments chemistry Pruthi, J. S.
  9. Food Technology v.48 Spices and seasoning blends Giese, J.
  10. Perfumer and Flavorist v.8 A review of oleoresin black pepper and its extraction solvents Pagington, J. S.
  11. Spices, condiments and seasonings Farrell, K. T.
  12. 부산대학교대학원 석사학위논문 초피나무의 휘발성 성분 및 항균력에 관한 연구 권선진
  13. 한국음식문화연구원논문집 방향과 식물 종실의 항산화성 물질에 관한 연구 조용계
  14. The essential oils Guenther, E.
  15. Bull. Jpn. Soc. Sci. Fisheries v.24 On the volatile components of Zanthoxylum piperitum DC Katayama, T.
  16. Bull. Chem. Soc. Jpn. v.41 Constituents of fruit oil from Japanes pepper Sakai, T.;Yoshihara, K.;Hirose, Y.
  17. 한국영양학량학회지 v.16 천초에 관한 연구 ; 1. 향미성분과 정유성분 정현숙
  18. 한국식품과학회지 v.21 초피의 과피와 잎의 방향성분 김정환;이경석;오원택;김경례
  19. J. Agr. Food Chem. v.25 Isolation of volatile components from a model system Schults, T. H.;Flath, R. A.;Mon, T. R.;Eggling, S. B.;Teranishi, R.
  20. 기기분석 김승재;서성규
  21. Perfumer & Flavorist v.13 Production of rosemary oleoresin using supercritical carbon dioxide Tateo, F.;Fellin, M.
  22. 한양대학교대학원 박사학위논문 한국산 초피와 산초와 과피 및 종실의 성분에 관한 연구 한희자