A Study on Synthesis of (Mo.W)$\textrm{Si}_2$ Composites

이규화몰리.텅스텐 복합재료의 합성에 관한 연구

  • Jang, Dae-Gyu (Minerals Utilization Division, Korea Institute of Geology, Mining & Materials) ;
  • Abbaschian, R. (Dept. of Materials Science and Engineering, University of Florida)
  • 장대규 (한국자원연구소 활용연구부) ;
  • Published : 1999.01.01

Abstract

(Mo.W)Si$_2$ composites were fabricated by vacuum hot-pressing elemental Mo, W and Si powders at various temperatures. Elemental Mo, W and Si powders were alloyed in the proper proportions to form solid solutions. The microstructure and properties of these materials was characterized by using x-ray diffraction, optical microscopy, energy dispersive x-ray spectroscopy and Vicker's technique. It was found that tungsten was mainly substituted for Mo atoms, and made a completed solid solution of (Mo.W)Si$_2$ over 1$600^{\circ}C$. The lattice parameters and Vickers hardness increased largely with increasing reaction temperature by the most soluble elements, due to the solid-solution hardening.

Keywords

References

  1. report RM E9G01(1949),RME52A04(1952), and E52D09, National Advisory Committe for Aeronautics W.A.Maxwell
  2. Swedish Patent Number v.155 Kanthal
  3. 한국재료학회지 v.7 no.9 이규화몰리브덴 고온 발열체의 제조에 관한 연구 김원백;장대규;심건주;서창열
  4. Mater. Sci. and Eng. v.A144 L.Xiao;Y.S.Kim;R.Abbaschian
  5. Materials Science and Engineering v.A155 R.B.Schwarz;S.R.Srinivasan;J.J.Petrovic;C.J.Maggiore
  6. Scripta Materialia v.34 no.8 D.E.Alman;R.D.Govier
  7. J. Am. Ceram. Soc. v.79 no.7 I.J.Shon;Z.A.unir;K.Yamazaki;K.Shoda
  8. Mater. Sci. and Eng. v.A149 Seetharama C. Deevi
  9. Ceram. Eng. Sci. Proc. v.12 J.J.Petrovic;R.E.Honnel;T.E.Mitchell
  10. Mater. Sci. Eng. v.A155 L.Xiao;R.Abbaschian
  11. Whicker and Fiber-toughened ceramics E.Fitzer;R.A.Bradley(ed.)D.E.Clark(ed.)D.C.Larsen(ed.)J.O.Stiegler(ed.)
  12. J. Mater. Sci. v.25 K.Kimura;M.Nakamura;T.Hirano
  13. J. Japan Ins. Metal v.58 no.11 Yoshihisa Harada;Yasufumi Funato;Masahiko Morinaga
  14. Master's Thesies, University of Florida, Dept. of Materrials Science and Engineering A.Gomez
  15. Certif. 255221, 1170735 Synthesis of refractory Inorganic Compounds Merzhanov, A.G.;Borovinskaya, I.P.
  16. Trans. Faraday Soc. v.19 A.L.Norbury