Journal of the Korean Society of Food Science and Nutrition (한국식품영양과학회지)

The Korean Society of Food Science and Nutrition (한국식품영양과학회)
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Chemical Synthesis of Conjugated Linoleic Acid (CLA) Derivatives with Glycerol

Conjugated Linoleic Acid (CLA) Glycerol 유도체의 화학적 합성

  • Published : 2000.06.01
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Abstract

CLA의 glycerol 유도체를 화학적으로 합성하였다. CLA-Cl(1.79 mmole), glycerol(0.6 mmole)과 pyridine (1.3mL)를 25C에서 8시간 반응시켰다. 이 반응물을 SGCC와 TLC를 이용하여 CLA의 glycerol 유도체를 분리하고 1H-NMR, 13C-NMR, IR, MS를 이용하여 분리된 유도체를 동정하였다. 이 실험조건하에서 사용된 CLA의 59.4%가 CLA의 glycerol 유도체(CLA-TG, CLA-DG, CLA-MG)로 전환되었다. CLA의 glycerol 유도체 중 CLA-TG는 52.1%, CLA-DG는 17.0%, CLA-MG는 30.9%였다.

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References

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