Synthesis of Nanosized $CeO_2$Powders by Hydrothermal Process

  • Bae, Dong-Sik (Division of Ceramics, Korea Institute of Science & Technology) ;
  • Paek, Yeong-Kyeun (Department of Materials Science & Engineering, Andong National University)
  • Published : 2001.11.01

Abstract

Nanosized CeO$_2$Powders were prepared under high temperature and pressure conditions by precipitation from metal nitrates with aqueous potassium hydroxide. Spherical shape of CeO$_2$powder was obtained at 175$^{\circ}C$ for 6h. TEM and X-ray diffraction patterns showed that the synthesized particle was crystalline. The average size and size distribution of the synthesized particles were below 30 nm and narrow, respectively. In addition, the effects of synthesis parameters under hydrothermal process are discussed.

Keywords

References

  1. J. Am. Ceram. Soc. v.79 no.3 Hydrothermal Synthesis of Cerium (Ⅳ) Oxide M. Hirano;E. Kato
  2. J. Am. Ceram. Soc. v.76 no.6 Reactive Cerium (Ⅳ) Oxide Powders by the Homogeneous Precipitation Method P.L. Chen;I-W. Chen
  3. Am. Ceram. Soc. Bull. v.66 no.9 Hydrothermal Processing of Ceramics S. Hirano
  4. Am. Ceram. Soc. Bull. v.67 no.10 Hydrothermal Synthesis of Advanced Ceramic Powders W. J. Dawson
  5. Sci. Tech. & App. of Colloid. Susp Morphological Control of α-Al₂O₃Particles Precipitated from 1,4-butanediol Solution S. B. Cho;S. Venigalla;J. H. Adair;James H. Adair(ed.);Jon A. Casey(ed.);Clive A. Randall(ed.);Sridhar Venigalla(ed.)
  6. Euro-Ceramics v.5 Sintering of Nanosized MnZn Ferrite Powders M. Rozman;M. Drofenik;D. Kolar
  7. J. Am. Ceram. Soc. v.71 no.1 Hydrothermal Preparature of Ultrafine Ferrites and Their Sintering S. Komarneni;E. Freagan;E. Bravel;R. Roy
  8. Chem. Mater. v.7 no.4 Hydrothermal Preparation of Uniform Nanosize Rutile and Anatase Particles H. Cheng;J. Ma;Z. Zhao;L. Qi
  9. J. Am. Ceram. Soc. v.64 no.12 Hydrothermal Preparation of Ultrafine Monoclinic ZrO₂Powders E. Tani;M. Yoshimura;S. Somiya