Journal of the Korean Society of Food Science and Nutrition (한국식품영양과학회지)

The Korean Society of Food Science and Nutrition (한국식품영양과학회)
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Analysis of Radiolytic Compounds of Lipids for the Detection of Irradiation in Dried Mytilus coruscus

건조 홍합의 방사선 조사여부를 확인하기 위한 지방분해산물 분석

  • Lee, Hae-Jung (Dept. of Food and Nutrition, Chosun University) ;
  • Yun, Il-Nam (Dept. of Food and Nutrition, Chosun University) ;
  • Seo, Hye-Young (Dept. of Food and Nutrition, Chosun University) ;
  • Song, Hyun-Pa (Dept. of Food and Nutrition, Chosun University) ;
  • Hong, Chul-Hee (Dept. of Hotel and Food Service Industry, Suncheon Cheongam College) ;
  • Kim, Kyong-Su (Dept. of Food and Nutrition, Chosun University)
  • 이해정 (조선대학교 식품영양학과) ;
  • 윤일남 (조선대학교 식품영양학과) ;
  • 서혜영 (조선대학교 식품영양학과) ;
  • 송현파 (조선대학교 식품영양학과) ;
  • 홍철희 (순천청암대학 호텔외식산업과) ;
  • 김경수 (조선대학교 식품영양학과)
  • Published : 2002.08.01
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Abstract

Radiolytic compounds of lipids, as hydrocarbons and 2-alkylcyclobutanones, were determined to detect the irradiated dried Mytilus coruscus. The detection methods were composed of fat extraction by Soxtec apparatus from dried Mytilus coruscus, isolation of hydrocarbons and 2-alkylcyclobutanones with a florisil column chromatography and identification of GC/MS. Concentrations of the radiation-induced hydrocarbons and 2-alkylcyclobutanones increased with the irradiation dose. The major hydrocarbons in irradiated Mytilus coruscus were pentadecane and 1-tetradecene originated from palmitic acid, and heptadecane and 1-hexadecene originated from stearic acid. 2-(5'- Tetradecenyl)cyclobutanone of 2-alkylcyclobutanones was high relatively. The radiation - induced hydrocarbons and 2-alkylcyclobutanones from dried Mytilus coruscus were detected at 0.5 kGy over and not detected at the non-irradiated.

건조된 홍합을 방사선 조사시켜 생성된 hydrocarbon류를 분리하기 위하여 Soxtec기기를 이용하여 지방을 추출한 뒤, florisil column chromatography하였으며, GC/MS 분석기기로 성분을 확인하였다 0.5~10 kGy의 선량별로 조사된 건조된 홍합에서 방사선 조사에 의해 생성된 hydrocarbon류 함량이 조사선량에 따라 증가하였으며, 동일한 선량으로 조사된 시료임에도 방사선 조사에 의해 생성된 hydrocarbon류 각각의 함량이 다르게 정량되었다. 건조된 홍합의 방사선 조사에 의해 생성되는 hydrocarbon류와 2-alkylcyclobutanone류는 0.5 kGy 이상 조사된 시료에서 모두 검출되었으며, 비조사 시료에서는 검출되지 않았다.

Keywords

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