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The Effect of Solidification Rates and Thermal Gradients on Directionally Solidified Microstructure in the Ni-base Superalloy GTD111M

GTD111M 초내열합금에서 응고속도 및 온도구배가 일방향응고 조직 에 미치는 영향

  • Ye, Dae-Hee (Dept. of Metallurgy and materials Science, Changwon National University) ;
  • Kim, Cyun-Choul (Dept. of Metallurgy and materials Science, Changwon National University) ;
  • Lee, Je-Hyun (Dept. of Metallurgy and materials Science, Changwon National University) ;
  • Yoo, Young-Soo (Dept. of Mateials Processing, Korea Institute of machinery and Materials) ;
  • Jo, Chang-Yong (Dept. of Mateials Processing, Korea Institute of machinery and Materials)
  • 예대희 (창원대학교 금속재료공학과) ;
  • 김현철 (창원대학교 금속재료공학과) ;
  • 이재현 (창원대학교 금속재료공학과) ;
  • 유영수 (한국기계연구원 재료공정연구부) ;
  • 조창용 (한국기계연구원 재료공정연구부)
  • Published : 2002.12.01

Abstract

Morphological evolution and growth mechanism at the solid/liquid interface during solidification were investigated in the Ni-base superalloy GTD111M by directional soldification and quenching(DSQ) technique. The experiments were conducted by changing solidification rate(V) and thermal gradient(G) which are major solidification process variables. High thermal gradient condition could be obtained by increasing the furnace temperature and closely attaching the heating and cooling zones in the Bridgeman type furnace. The dendritic/equiaxed transition was found in the G/V value lower than $0.05$\times$10{^3}^{\circ}C$s/$\textrm{mm}^2$, and the planar interface of the MC-${\gamma}$ eutectic was found under $17 $\times$ 10{^3}^{\circ}C$ s/$\textrm{mm}^2$. It was confirmed that the dendrite spacing depended on the cooling rate(GV), and the primary spacing was affected by the thermal gradient more than solidification rate. The dendrite lengths were decreased as increasing the thermal graditne, and the dendrite tip temperature was close to the liquidus temperature at $50 \mu\textrm{m}$/s.

Keywords

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