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Nanoindentation Investigation of Mechanical Properties in Oxide Laminar Composites

Nanoindentation을 이용한 산화물 층상 복합체의 기계적 성질 평가

  • Published : 2003.07.01

Abstract

Tape cast laminar composites with alumina/zircon(reaction-bonded mullite/zirconia) as an inner layer and alumina/zirconia or mullite/zirconia as an outer layer have been fabricated by hot-pressing. The mechanical properties(hardness and Young's modulus) and microstructure of laminar composites were examined using a nanoindentation technique and Scanning Electron Microscopy (SEM), respectively. The indentation load-displacement curve revealed the existence of residual stress in laminar composites.

테이프 캐스팅법을 이용하여 알루미나/지르콘(반응결합 뮬라이트/지르코니아 유도)을 내부층으로 하고 알루미나/지르코니아 혹은 뮬라이트/지르코니아를 외부층으로 하는 산화물 층상 복합체를 고온가압소결법으로 제조하였다. 나노압입시험법을 이용하여 층상 산화물 복합체의 기계적 성질(경도 및 탄성계수)을 측정하고, SEM을 통하여 복합체의 미세구조를 관찰하였다. 산화물 층상 복합체의 제조를 위한 가열·냉각시 유도된 구성 산화물간의 열팽창 계수의 차이로 인하여 생성된 잔류응력을 하중-변위곡선을 이용하여 확인할 수 있었다.

Keywords

References

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