DOI QR코드

DOI QR Code

Effect of Annealing for YIG Single Crystal Thick Films

YIG 단결정 후막의 열처리의 효과

  • 김근영 (성균관대학교 신소재공학과) ;
  • 윤석규 (성균관대학교 신소재공학과) ;
  • 김용탁 (성균관대학교 신소재공학과) ;
  • 이성문 (성균관대학교 신소재공학과) ;
  • 윤대호 (성균관대학교 신소재공학과)
  • Published : 2003.09.01

Abstract

When the PbO-based flux system is used in the Liquid Phase Epitaxy (LPE) method for Yttrium Iron Garnet (YIG) thick film, the effect of Pb ions incorporated into the grown crystal; increase the lattice parameter, changed the uniaxial magnetic anisotropy constant (Ku) or conductance of grown film. It exerts a bad influence on physical property such as increasing optical absorption of grown film. The content of the Pb ion in crystal was decreased by volatilization of Pb ion after annealing; therefore, the lattice parameter of film was reduced on an average 0.0115 ${\AA}$ by the the Pb ion.

Liquid Phase Epitaxy (LPE)법으로 Yttrium Iron Garnet (YIG:Y$_3$Fe$_{5}$O$_{12}$) 단결정 후막을 성장시킬 때 PbO계 응제에서는 Pb 이온이 성장되는 결정내로 혼입되어 성장된 막의 격자상수를 증가시키고, 일축 자기이방성 상수값(Ku)을 변화시키거나 전기 전도도를 변화시킨다. 또한 광 흡수율을 증가시키는 등의 성장된 막의 물성에 악영향을 미친다. 열처리 후 Pb 이온의 휘발로 인한 결정내의 농도감소로 성장된 단결정 후막의 격자상수가 평균 0.0115$\AA$ 감소하였다.

Keywords

References

  1. Physics of Garnet A.Paoletti
  2. Microwave Magnetics R.F.Soohoo
  3. The J. Kor. Inst. Elect. Mater. Eng. v.9 no.1 The Present Technical Condition and a Trend of Research for Soft Magnetic Materials Y.K.Park;K.J.Yang
  4. J. Cryst. Growth v.42 Growth of Magnetic Garnet Single Crystals from High Temperature Solution W.Tolksdorf https://doi.org/10.1016/0022-0248(77)90206-8
  5. Appl. Phys. Lett. Growth of High-quality Garnet Films from Supercooled Melts H.J.Levinstein;S.Licht;R.W.Landorf;S.L.Blank
  6. J. Cryst. Growth v.27 Stress Relief in Magnetic Garnet Films Grown by Liquid Phase Epitaxy D.C.Miller;R.Caruso https://doi.org/10.1016/S0022-0248(74)80074-6
  7. IEEE Trans. Magn. v.23 no.5 Narrow FMR Linewidth Dependence on Growth Conditions in LPE YIG Films J.M.Desvignes;D.Mahasoro;H.L.Gall https://doi.org/10.1109/TMAG.1987.1065740
  8. J. Kor. Ceram. Soc. v.39 no.6 Growth of Bi:YIG Thick Films by Change of PbO/Bi₂O₃Molar Ratio S.G.Yoon;G.Y.Kim;Y.T.Kim;H.M.Jung;Y.M.Im;D.H.Yoon https://doi.org/10.4191/KCERS.2002.39.6.589
  9. J. Cryst. Growth v.17 The Growth of Magnetic Garnets by Liquid Phase Epitaxy S.L.Blank;J.W.Nielsen https://doi.org/10.1016/0022-0248(72)90261-8
  10. J. Cryst. Growth v.27 Accomodation of Pb in Yttrium Iron Garnet Films Grown by Liquid Phase Epitaxy H.L.Glass;M.T.Elliott
  11. J. Appl. Phys. v.48 no.3 Pb Valence in Iron Garnets G.B.Scott;J.L.Page https://doi.org/10.1063/1.323728