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Effect of Sintering Atmosphere Changing Temperature on Microstructure and Mechanical Property of Al2O3/Cu Nanocomposites

소결분위기 변환온도가 Al2O3/Cu 나노복합재료의 미세조직과 파괴강도에 미치는 영향

  • Oh Sung-Tag (Dept. of Materials Science and Engineering, Seoul National University of Technology) ;
  • Yoon Se-Joong (Dept. of Materials Science and Engineering, Seoul National University of Technology)
  • 오승탁 (서울산업대학교 신소재공학과) ;
  • 윤세중 (서울산업대학교 신소재공학과)
  • Published : 2004.10.01

Abstract

The microstructure and mechanical property of hot-pressed $Al_2O_3/Cu$ composites with a different temperature for atmosphere changing from H$_{2}$ to Ar have been studied. When atmosphere-changed from H$_{2}$ to Ar gas at 145$0^{\circ}C$, the hot-pressed composite was characterized by inhomogeneous microstructure and low fracture strength. On the contrary, when atmosphere-changed at low temperature of 110$0^{\circ}C$ the composite showed more homogeneous microstructure, higher fracture strength and smaller deviation in strength. Based on the thermodynamic consideration and microstructural analysis, it was interpreted that the Cu wetting behavior relating to the formation of CuAlO$_{2}$ is probably responsible for strong dependence of microstructure on atmosphere changing temperature. The reason for a strong sensitivity of fracture strength and especially of its deviation to atmosphere changing temperature was explained by the microstructural inhomogeneity and by the role of CuAlO$_{2}$ phase on the interfacial bonding strength.

Keywords

References

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