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Indentation Damage of Porous Alumina Ceramice

  • Ha, Jang-Hoon (Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology) ;
  • Lee, Chul-Seung (Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology) ;
  • Kim, Jong-Ho (Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology) ;
  • Kim, Do-Kyung (Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology)
  • Published : 2004.01.01

Abstract

The Hertzian indentation contact damage behavior of porous alumina with controlled pore shape was investigated by experiments. Porous alumina ceramics containing well-defined pore shape, size and distribution were prepared by incorporation of fugitive spherical starch. Porous alumina with isolated pore structure was prepared with porosity range up to 30%. The indentation stress-strain curves of porous alumina were constructed. Elastic modulus and yield stress can be obtained from the stress-strain relationship. Impulse excitation method for the measurement of elastic modulus was also conducted as well as Hertzian indentation and was confirmed as a useful tool to evaluate the elasticity of highly porous ceramics. Elastic modulus of the inter-connected pore structure is more sensitive to porosity than that of the isolated pore structure. When the specimen had isolated pore structure, higher yield point was obtained than it had inter-connected pore structure. This study proposed that the elastic modiulus of porous ceramics is strongly related to not only porosity, but also the structure of pore.

Keywords

References

  1. R. L. Coble and W. D. Kingery, 'Effect of Porosity on Physical Properties of Alumina,' J. Am. Ceram. Soc., 39 [11] 377-85 (1956) https://doi.org/10.1111/j.1151-2916.1956.tb15608.x
  2. Z. Hashin, 'The Elastic Moduli of Heterogeneous Materials,' J. Appt. Mech., 29 [1] 143-50 (1962) https://doi.org/10.1115/1.3636446
  3. N. Ramakrishnan and V. S. Arunachalam, 'Effective Elastic Moduli of Ceramic Materials,' J. Am. Ceram. Soc., 76 [10] 2745-52 (1993) https://doi.org/10.1111/j.1151-2916.1993.tb04011.x
  4. J. Y. Yun, H. D. Kim, and C. H. Park, 'Fabrication of Double-layered Porous Materials,' J. Kor. Ceram. Soc., 39 [10] 919-27 (2002) https://doi.org/10.4191/KCERS.2002.39.10.919
  5. A. R. Boccaccini and Z. Fan, 'A New Approach for the Young's Modulus-porosity Correlation of Ceramic Materials,' Ceram. Int., 23 239-45 (1997) https://doi.org/10.1016/S0272-8842(96)00033-8
  6. A. P. Roberts and E. J. Garboczi, 'Elastic Moduli of Model Random Three-dimensional Closed-cell Cellular Solids,' Acta Mater., 189-97 (2001)
  7. A. P. Roberts and E. J. Garboczi, 'Elastic Properties of Model Random Three-dimensional Open-cell Solids,' J. Mech. Phys. Solids, 50 33-55 (2002) https://doi.org/10.1016/S0022-5096(01)00056-4
  8. R. W. Rice, 'Porosity of Ceramics,' Marcel Dekker, Inc., New York, p. 20 (1997)
  9. B. R. Lawn, 'Indentation of Ceramics with Spheres : A Century after Hertz,' J. Am. Ceram. Soc., 81 [8] 1977-94 (1998) https://doi.org/10.1111/j.1151-2916.1998.tb02580.x
  10. J. She, J. F. Yang, Y. Beppu, and T. Ohji, 'Hertzian Contact Damage in a Highly Porous Silicon Nitride Ceramic,' J. Eur. Ceram. Soc., 23 1193-97 (2003) https://doi.org/10.1016/S0955-2219(02)00301-1
  11. K. S. Lee, D. K. Kim, S. K. Woo, and M. H. Han, 'Strength Degradation from Contact Fatigue in Self-toughened Glass-ceramics,' J. Kor. Ceram. Soc., 7 [2] 63-9 (2001)
  12. 'Standard Test Method For Dynamic Young's Modulus, Shear Modulus and Poisson's Ratio by Impulse Excitation of Vibration' ASTM, E1876-1
  13. B. A. Latella, B. H. O'Connor, N. P. Padture, and B. R. Lawn, 'Hertzian Contact Damage in Porous Alumina Ceramics,' J. Am. Ceram. Soc., 80 [4] 1027-31 (1997) https://doi.org/10.1111/j.1151-2916.1997.tb02940.x
  14. R. W. Rice, 'Evaluation and Extension of Physical Property-porosity Models Based on Minimum Solid Area,' J. Mater. Sci., 31 102-18 (1996) https://doi.org/10.1007/BF00355133
  15. E. A. Dean and J. A. Lopez, 'Empirical Dependence of Elastic Moduli on Porosity for Ceramic Materials,' J. Am. Ceram. Soc., 60 [7-8] 345-49 (1977) https://doi.org/10.1111/j.1151-2916.1977.tb15558.x
  16. F. P. Knudsen, 'Effect of Porosity on Young's Modulus of Alumina,' J. Am. Ceram. Soc., 45 [2] 94-5 (1962) https://doi.org/10.1111/j.1151-2916.1962.tb11089.x
  17. R. M. Spriggs, 'Effect of Open and Closed Pores on Elastic Moduli of Polycrystalline Alumina,' J. Am. Ceram. Soc., 45 [9] 454 (1962) https://doi.org/10.1111/j.1151-2916.1962.tb11192.x

Cited by

  1. Strength and Reliability of Porous Ceramics Measured by Sphere Indentation on Bilayer Structure vol.41, pp.7, 2004, https://doi.org/10.4191/KCERS.2004.41.7.503