Journal of the Korean Ceramic Society (한국세라믹학회지)

The Korean Ceramic Society (한국세라믹학회)
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Effect of MgO Diluents in Combustion Synthesis of TiB2 Nano Particles

TiB2 나노 입자의 연소합성 시 MgO 희석제가 미치는 영향

  • Lee, Byung-Ki (Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology) ;
  • Lee, Jong-Moo (Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology) ;
  • Park, Je-Hyeong (Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology) ;
  • Kang, Eul-Son (Agency for Defense Development) ;
  • Baek, Seung-Soo (Agency for Defense Development) ;
  • Kim, Do-Kyung (Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology)
  • 이병기 (한국과학기술원 신소재공학과) ;
  • 이종무 (한국과학기술원 신소재공학과) ;
  • 박제형 (한국과학기술원 신소재공학과) ;
  • 강을손 (국방과학연구소) ;
  • 백승수 (국방과학연구소) ;
  • 김도경 (한국과학기술원 신소재공학과)
  • Published : 2005.09.01
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Abstract

The effect of MgO diluents in combustion synthesis of $TiB_2$ nano particles was investigated. The reaction $TiO_2\;+\;B_2O_3\;+\;xMg\;{\rightarrow}\;TiB_2\;+\;5MgO$ was used to synthesize $TiB_2$ nano particles. The combustion velocity was measured to examine the relation between the reaction temperature and the morphologies of particles. The diluent MgO did not react with the reactants and played a role to decrease combustion temperature. As the MgO diluents contents increased, the particles with the smaller size and the narrower size distribution were synthesized. At the condition of 6 mole of MgO, the combustion wave velocity was about 5 cm/see and the synthesized particles showed the size of 60 nm with narrow size distribution.

Keywords

References

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