Changes of Volatile Compounds in Flue-cured Leaf Tobacco during Aging

황색종 잎담배의 후숙과정 중 정유성분의 변화

  • 복진영 (KT&G 중앙연구원) ;
  • 박윤신 (국립과학수사연구소 중부분소) ;
  • 박원종 (공주대학교 산업과학대학 식품공학과) ;
  • 이종률 (KT&G 중앙연구원)
  • Published : 2006.12.31

Abstract

This study was carried out to investigate the changes of essential oils in flue-cured leaf tobacco during aging for 21 months. The threshed leaf tobacco(BlO) produced in 2002 crop year was aged for 21 months in the warehouse of Oc-Cheon Leaf Tobacco Processing Factory. The leaf tobacco were sampled at three month intervals for analysis of volatile compounds. Volatile compounds were identified by GC/MS and comparison of gas chromatographic retention time with those of the authentic standard. The total of 75 compounds from the steam volatile concentrate of the flue-cured leaf tobacco were identified; they were 15 hydrocarbons, 12 alcohols, 3 aldehydes, 18 ketones, 7 esters, 10 acids, 3 phenols, 4 furans, 2 pyrrols and 1 pyridine. The major components of essential oil were neophytadiene, solanone, megastigmatrienone and phytol. After a aging period of 21 months, most of volatile compounds showed a gradual increasing tendency.

Keywords

References

  1. Burton, H. R., Bush, L. P. and Hamilton, J. L. (1983) Effect of curing on the chemical composition of burley tobacco. Rec. Adv. Tob. Sci. 9: 91-53
  2. Chortyk, O. T., Serverson, R. F. and Higman, H. C. (1975) Chromatographic determination of hydrocarbon waxes in tobacco leaf and smoke. Beit. Tabakforsch 8: 204-210
  3. Enzell, C. R. (1976) Terpenoid components of leaf and their relationship to smoking quality and aroma. Rec. Adv. Tob. Sci. 2: 32-60
  4. Enzell, C. R., Wahlberg, I. and Aasen A. J. (1977) Isoprenoids and alkaloids of tobacco. Progress Chem. Org. Natural Products 34: 1-79
  5. Enzell, C. R. and Wahlberg, I. (1980) Leaf composition in relation to smoking quality and aroma. Rec. Adv. Tob. Sci. 6: 64-122
  6. Ivanov, I. and Ognyanov, I. (1966) On resin in Bulgarian oriental tobacco. Proceedings of 4th International Tobacco Scientific Congress. 779-785
  7. Laffingwell, J. C. (1976) Nitrogen components of leaf and their relationship to smoking quality and aroma. Rec. Adv. Tob. Sci. 2: 1-31
  8. Roberts, D. L. (1988) Natural tobacco flavor. Rec. Adv. Tob. Sci. 14: 49-81
  9. Sakai, T., Fukuhara, K., Niino, K. Sakuma, M. and Sugawara, S. (1985) Changes in the composition of headspace volatiles of flue-cured tobacco by aging. Agric. Biol. Chem. 49(6): 1785-1791 https://doi.org/10.1271/bbb1961.49.1785
  10. Schultz, T. H., Flath, R. A., Mon, T.R. and Teranishi, R. (1977) Isolation of volatile components from a model system. J. Agric. Food Chem. 25: 466-471 https://doi.org/10.1021/jf60211a031
  11. Wahlberg, I., Karlsson, K., Austin, D. J., Junker, N., Roeraade, J. and Enzell, C. R. (1977) Effect of flue-curing and ageing on the volatile, neutral and acidic constituents of virginia tobacco. Phytochemistry 16: 1217-1231 https://doi.org/10.1016/S0031-9422(00)94363-2
  12. Weeks, W. W. (1985) Chemistry of tobacco constituents influencing flavor and aroma. Rec. Adv. tob. Sci. 11: 175-200
  13. 宇井信生 (1984), 生化學辭典, p691. 東京化學同人, 日本
  14. 김경례, 박진우, 허일 (1981) 향끽미종 잎담배 성분 조성에 관한 연구. III. 정유성분의 특성 조사. 한국연초학회지 3(1): 11-19
  15. 김신일, 오영일, 허일 (1983) 잎담배의 중요 휘발성 정유성분 분석. 한국연초학회지 5(2): 47-54
  16. 석영선 (1988) 열풍 건조조건에 따른 황색종 연초엽의 이화학성 변화. 충북대학교 박사학위 논문
  17. 이경구, 박진우 (1982) 담배 이분중 Essential Oil의 활용 연구. 한국연초학회지 4(2): 67-73
  18. 장기운 (1985) 한미산 황색종 잎담배의 휘발성 정유성분 비교 연구. 한국연초학회지 7(2): 151-167
  19. 정기택, 안대진, 이종률, 제병권 (2004) 황색종 잎담배의 숙성기간이 색상, 화학성분 및 끽미에 미치는 영향. 한국연초학회지 26(1): 27-34
  20. 지상운 (1997) 황색종 잎담배의 건조과정에서 성분 변화. 상지대학교 박사학위 논문