The Shear Bond Strength of Resin to Electroforming Gold according to the Surface Treatment

표면처리방법에 따른 Electroforming Gold와 레진과의 전단결합강도

  • You, Byung-Il (Department of Prosthodontics, and Institute of Oral Bio-Science, School of Dentistry, Chonbuk National University) ;
  • Chang, Mun-Suk (Department of Prosthodontics, and Institute of Oral Bio-Science, School of Dentistry, Chonbuk National University) ;
  • Yoon, Tae-Ho (Department of Prosthodontics, and Institute of Oral Bio-Science, School of Dentistry, Chonbuk National University) ;
  • Park, Ju-Mi (Department of Prosthodontics, and Institute of Oral Bio-Science, School of Dentistry, Chonbuk National University) ;
  • Park, Charn-Woon (Department of Prosthodontics, and Institute of Oral Bio-Science, School of Dentistry, Chonbuk National University)
  • 유병일 (전북대학교 치과대학 치과보철학교실, 구강생체과학연구소) ;
  • 장문숙 (전북대학교 치과대학 치과보철학교실, 구강생체과학연구소) ;
  • 윤태호 (전북대학교 치과대학 치과보철학교실, 구강생체과학연구소) ;
  • 박주미 (전북대학교 치과대학 치과보철학교실, 구강생체과학연구소) ;
  • 박찬운 (전북대학교 치과대학 치과보철학교실, 구강생체과학연구소)
  • Published : 2006.06.30

Abstract

Statement of problem. The success of the bonding between electroforming gold and resin is dependent on the surface-conditioning technique but its effective technique has net been studied widely. Purpose. The purpose of the study was to evaluate the bond strength between the electroforming gold and resin with varying the surface-conditioning technique. Materials and methods. Sixty rectangular shaped metal specimens were made and one side of each specimen were gold hard plated. The sand-blasted specimens were divided into four experimental groups with fifteen specimens in each group and were treated as follows. Group 1: Silicoating (Rocatec, 3M ESPE)+ Sinfony (3M ESPE), Group 2: SR Link+ SR Adoro (Ivoclar Vivadent), Group 3: Tin plating (Microtin, Danville Engineering)+ SR Link+ SR Adoro, Group 4: Tin plating (Micro tin, Danville Engineering)+ Silicoating (Rocatec)+ Sinfony. Shear bond strength at metal-resin interface were measured using universal testing machine. Energy Dispersive x-ray analysis was done and scanning electron microscope images were taken and observed. Results and Conclusion. The following conclusions were drawn. 1. The mean shear bond strength values in order were 11.69MPa (Group 2), 22.35MPa (Group 3), 22.40MPa (Group 1) and 27.71MPa (Group 4). There was no significant difference in Group 1, Group 3 and Group 4(P>0.05). 2. In the EDX line analysis, the Au was detected on the surface of all specimen. $SnO_2$ showed on the surface of Group 2 and $SiO_2$ was detected on the surface of Group 1. 3. Increasing of roughness by sandblasting(Group 2), formation of micro-irregularities and tin crystals by electrolytic tin plating(Group 3) and formation of surface irregularities and $SiO_2$ layer(Group 1,4) were observed in SEM photo. 4. Tin plating(Group 3) and Rocatec treatment(Group 1) showed clinically effective shear bond strength(>20MPa), but when the two surface conditioning method were used together higher bond strength were achieved.

Keywords

References

  1. Mahler DB, Ady AB. An explanation for the hygroscopic setting expansion of dental gypsum products. J Dent Res 1960;39:578-89 https://doi.org/10.1177/00220345600390031901
  2. Yamamoto M. Metal-ceramics. Quintessence Pub. Co. Tokyo, 1985
  3. Campbell SD, Sozio RB. Evaluation of the fit and strength of an all-ceramic fixed partial denture. J Prosthet Dent 1988;59:301-6 https://doi.org/10.1016/0022-3913(88)90177-1
  4. Chan C, Haraszthy G, Geis-Gerstorfer J, Weber H, Huettemann H. Scanning electron microscopic studies of the marginal fit of three esthetic crowns. Quintessence Int 1989;20: 189-93
  5. Rinke S. Fitting accuracy of FPDs produced by a CAD/CAM system for the production of metal copings for porcelain-fused-to-metal restorations. J Dent Res 1996;75:138-43
  6. Raigrodski AJ, Malcamp C, Rogers WA. Electroforming teclmique. J Dent Technol 1998;15: 13-6
  7. Behrend F. Gold Electroforming System: GES restorations. J Dent Technol 1997;14:31-7
  8. Holmes JR, Pilcher ES, Rivers JA, Stewart RM. Marginal fit of electroformed ceramometal crowns. J Prosthodont 1996;5:111-114 https://doi.org/10.1111/j.1532-849X.1996.tb00284.x
  9. Setz J, Diehl J, Weber H. The marginal fit of cemented galvanoceramic crowns. Int J Prosthodont 1989;2:61-4
  10. Petteno D, Schierano G, Bassi F, Bresciano ME, Carossa S. Comparison of marginal fit of 3 different metal-ceramic systems: an in vitro study. Int J Prosthodont 2000;13:405-8
  11. Wirz J, Hoffman A. Electroforming in restorative dentistry: new dimensions in biologically based prostheses. Quintessence Pub. Co. 1999
  12. Raigrodski AJ, Malcamp C, Rogers WA. Electroforming teclmique. J Dent Technol 1998;15: 13-6
  13. Jacques LB, Ferrari M, Cardoso PE. Microleakeage and resin cement film thickness of luted all-ceramic and gold electroformed porcelain-fused-to-metal crowns. J Adhes Dent 2003;5:145-52
  14. Metal resin bonding. Adept report 1991;30:418-423
  15. Raigrodski AJ, Malcamp C, Rogers WA. Electroforming teclmique. J Dent Technol 1998; 15:13-6
  16. Kwon HB, Yim SH. A qualitative analysis of bonding between electroformed surface and veneering ceramics. J Korea Acad Prosthodont 2000;38:328-35
  17. Tiller HJ, Gobel R, Magnus B, Musil R, Garschke A, Lockowandt P,Oden A. Sandblasting procedures and its effect on the surface properties of dental alloys (II). Quintessenz 1985;36:2151-8
  18. van der Veen JH, Jongebloed WL, Dijk F, PurdellLewis DJ, van de Poel AC. SEM study of six retention systems for resin-to-metal bonding. Dent Mater 1988;4:266-71 https://doi.org/10.1016/S0109-5641(88)80021-6
  19. van der Veen JH, Bronsdijk AE, Siagter AP, van de Poel AC, ArendsJ. Tensile bond strength of Comspan resin to six differently treated metal surfaces. Dent Mater 1988;4:272-7 https://doi.org/10.1016/S0109-5641(88)80022-8
  20. van der Veen JH, Bronsdijk AE, van de Poel AC. Resin-bondedbridges with tin-electroplated retainers results after three years.Ned Tijdschr Tandheelkd 1988;95:64-7
  21. Thompson VP, Del Castillo E, Livaditis GJ. Resin-bonded retainers.Part I: Resin bond to electrolytically etched nonprecious alloys. J Prosthet Dent 1983;50:771-9 https://doi.org/10.1016/0022-3913(83)90088-4
  22. Yamashita A. The clinical application of a new adhesive resin(MMA-4-META-TBB-O) to an adhesion bridge (adhesion splint). Shikai Tenbo 1982;59:671-82
  23. Yarnashita A. A new adhesive bridge. Nippon Shika Ishikai Zasshi 1983;35: 1074-87
  24. Gates WD, Diaz-Amold AM, Aquilino SA, Ryther JS. Comparison of the adhesive strength of a BIS-GMA cement to tin-plated and non-tin-plated alloys. J Prosthet Dent 1993;69:12-6 https://doi.org/10.1016/0022-3913(93)90232-D
  25. Guggenberger R. Rocatec system--adhesion by tribochemical coating. Dtsch Zalmarztl Z 1989;44: 874-6
  26. Marinello CP, Luthy H, Scharer P. Silicoater increases bonding strengthin the adhesive technique. Dent Labor 1990;38:1625-9
  27. Pfeiffer P. Chemical bond of adhesive and palladium alloys. ZWR 1991;100:292, 294, 297-8
  28. Tiller HJ. The silicoater MD-teclmique. A new version of the established silicoater technique. Zahntechni. 1991;48:28-30
  29. Watanabe F, Powers JM, Lorey RE. In vitro bonding of prosthodontic adhesives to dental alloys. J Dent Res 1988 ;67:479-83 https://doi.org/10.1177/00220345880670020901
  30. Luthy H, Marinello CP, Scharer P. Factors influencing metal-resin tensile bond strength to filled composites. Dent Mater 1990;6:73-7 https://doi.org/10.1016/S0109-5641(05)80033-8