Journal of the Korean Society of Food Science and Nutrition (한국식품영양과학회지)

The Korean Society of Food Science and Nutrition (한국식품영양과학회)
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Automatic Titration Using Micro pH Electrode in Volatile Basic Nitrogen Analysis

마이크로 pH전극을 이용한 휘발성염기질소의 자동적정

  • Published : 2006.04.01
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Abstract

An automatic titration was performed by a home-made automatic control system adopting a micro pH electrode as its sensing part in microdiffusion-based volatile basic nitrogen (VBN) analysis. The micro electrode was considered to be adequate for automatic VBN analysis because of its small sensor size, low immersion depth and unbreakable body. Six pork samples in different degree of freshness were analyzed both manually and automatically. The data from automatic titration were not significantly different from those taken by manual titration even at 15% significance level. The correlation coefficient was 1.000.

미량확산법에 의한 휘발성 염기질소 분석에서 고체소자센서가 부착된 마이크로 pH 전극을 사용하여 적정 과정을 자동화하기 위하여 자동적정시스템을 구성하고 자동적정 프로그램을 작성하였다. 자동적정시스템으로 돈육시료의 휘발성염기질소 분석을 수행한 결과 부패도가 서로 다른 모든 시료에서 자동적정과 수동적정의 평균들 간에 유의수준 15%에서도 유의차가 인정되지 않았으며, 두 방법의 평균치들 사이에 높은 상관성이 확인되었다.

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References

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