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Preparation and Characterization of SiC Coated Graphite Foam

SiC가 코팅된 그라파이트 Foam의 제조 및 특성 분석

  • Kyung, Jae-Jin (Eco-Materials Team, Korea Institute of Ceramic Engineering and Technology) ;
  • Kim, Jung-Ju (Eco-Materials Team, Korea Institute of Ceramic Engineering and Technology) ;
  • Kim, Soo-Ryong (Eco-Materials Team, Korea Institute of Ceramic Engineering and Technology) ;
  • Kwon, Woo-Teck (Eco-Materials Team, Korea Institute of Ceramic Engineering and Technology) ;
  • Cho, Kwang-Youn (Eco-Materials Team, Korea Institute of Ceramic Engineering and Technology) ;
  • Kim, Young-Hee (Eco-Materials Team, Korea Institute of Ceramic Engineering and Technology)
  • Published : 2007.11.30

Abstract

Graphite is widely used in electronic industry due to its excellent electrical and thermal properties. However, graphite starts to oxidize around $400^{\circ}C$ that seriously degrades its properties. SiC coating can be applied to graphite foam to improve its high temperature oxidation resistance. In this research, SiC coating on graphite foam was made via preceramic polymer using a polyphenylcarbosilane. 20% of polyphenylcarbosilane in hexane solution was coated onto graphite by dip coating method. Thermal oxidation was carried out at $200^{\circ}C$ for crosslink of the preceramic polymer and the sample were pyrolysized at $800^{\circ}C{\sim}1200^{\circ}C$ under nitrogen to convert the preceramic polymer to SiC film. The microstructure of the SiC coating after pyrolysis was investigated using FESEM and oxidation resistance up to $800^{\circ}C$ was evaluated.

Keywords

References

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Cited by

  1. Step-Growth Polymerization of Poly(phenylcarbosilane) and Its Structural and Physical Properties vol.22, pp.2, 2012, https://doi.org/10.1007/s10904-011-9624-1