Measurements of Two-dimensional Gratings Using a Metrological Atomic Force Microscope and Uncertainty Evaluation

길이 표준 소급성을 갖는 원자간력 현미경을 이용한 2차원 격자 시편 측정과 불확도 평가

  • 김종안 (한국표준과학연구원 기반표준부 길이/시간그룹) ;
  • 김재완 (한국표준과학연구원 기반표준부 길이/시간그룹) ;
  • 강주식 (한국표준과학연구원 기반표준부 길이/시간그룹) ;
  • 엄태봉 (한국표준과학연구원 기반표준부 길이/시간그룹)
  • Published : 2007.09.01

Abstract

The pitch and orthogonality of two-dimensional (2D) gratings have been measured by using a metrological atomic force microscope (MAFM) and measurement uncertainty has been analyzed. Gratings are typical standard artifacts for the calibration of precision microscopes. Since the magnification and orthogonality in two perpendicular axes of microscopes can be calibrated simultaneously using 2D gratings, it is important to certify the pitch and orthogonality of 2D gratings accurately for nano-metrology using precision microscopes. In the measurement of 2D gratings, the MAFM can be used effectively for its nanometric resolution and uncertainty, but a new measurement scheme was required to overcome some limitations of current MAFM such as nonnegligible thermal drift and slow scan speed. Two kinds of 2D gratings, each with the nominal pitch of 300 nm and 1000 nm, were measured using line scans for the pitch measurement of each direction. The expanded uncertainties (k = 2) of measured pitch values were less than 0.2 nm and 0.4 nm for each specimen, and those of measured orthogonality were less than 0.09 degree and 0.05 degree respectively. The experimental results measured using the MAFM and optical diffractometer were coincident with each other within the expanded uncertainty of the MAFM. As a future work, we also proposed another scheme for the measurements of 2D gratings to increase the accuracy of calculated peak positions.

Keywords

References

  1. Teague, E. C., 'Nanometrology,' Proc. AlP Conf. Scanned Probe Microscopy, Vol. 241, p. 371, 1991
  2. Carneiro, K., 'The need for metrology in nanotechnology,' Danish Institute of Fundamental Merology, p. 2, 2001
  3. Postek, M. T., Vladar, A. E., Jones, S. N. and Keery, W. J., 'Interlaboratory study on the lithographically produced scanning electron microscope magnification standard prototype,' Journal of Research of the National Institute of Standards and Technology, Vol. 98, No.4, pp. 447-467, 1993 https://doi.org/10.6028/jres.098.033
  4. Nakayama, Y., Okazaki, S. and Sugimoto, A., 'Proposal for a new submicron dimension reference for an e-beam metrology system,' Journal of Vacuum Science and Technology B, Vol. 6, Issue 6, pp. 1930-1933, 1988 https://doi.org/10.1116/1.584135
  5. Meli, F., Thalman, R. and Blattner, P., 'High precision pitch calibration of gratings using laser diffractometry,' 1st international conference and general meeting of the euspen society for precision engineering and nanometrology, pp. 252-255, 1999
  6. Kim, J. A., Kim, J. w., Park, B. C., Kang, C. S. and Eom, T. B., 'Measurement of grating pitch standards using optical diffractometry and uncertainty analysis,' Journal of the Korean Society for Precision Engineering, Vol. 23, No.8, pp. 72-79, 2004
  7. Meli, F. and Thalmann, R., 'Long-range AFM profiler used for accurate pitch measurements,' Meas. Sci. Technol., Vol. 9, No.7, pp. 1087-1092, 1998 https://doi.org/10.1088/0957-0233/9/7/014
  8. Misumi, I., Gonda, S., Kurosawa, T. and Takamasu, K., 'Uncertainty in pitch measurements of onedimensional grating standards using a nanometrological atomic force microscope,' Meas. Sci. Technol., Vol. 14, No.4, pp. 463-471, 2003 https://doi.org/10.1088/0957-0233/14/4/309
  9. Kim, J. A., Kim, J. W., Park, B. C., Eom, T. B. and Hong, J. W., 'Development of a metrological atomic force microscope for the length measurements of nanometer range,' Journal of the Korean Society for Precision Engineering, Vol. 21, No. 11, pp. 75-82, 2004
  10. Kim, J. A., Kim, J. W., Park, B. C., Eom, T. B. and Kang, C. S., 'Pitch measurement of one-dimensional gratings using a metrological atomic force microscope and uncertainty evaluation,' Journal of the Korean Society for Precision Engineering, Vol. 22, No.4, pp. 84-91,2005
  11. ISO, 'Guide to the Expression of Uncertainty in Measurement,' ISO, 1993