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Sn02 Two-dimensional Nanostructures Prepared by Solution Reduction Method and Their Gas Sensing Characteristics

용액환원법에 의한 Sn02 2차원 나노구조의 합성과 가스 감응 특성

  • Park, Hong-Chul (Department of Materials Science & Engineering, Korea University) ;
  • Kim, Hae-Ryong (Department of Materials Science & Engineering, Korea University) ;
  • Lee, Jong-Heun (Department of Materials Science & Engineering, Korea University)
  • Published : 2008.08.31

Abstract

SnO nanosheets were prepared at room temperature through a reaction between an aqueous solution of $SnCl_2$, $N_2F_4$, and NaOH and were converted into $SnO_2$ nanosheets without a morphological change. The SnO nanosheets were formed through a dissolution-recrystallization mechanism. Uniform and well-dispersed SnO nanosheets with the round-shape morphology were attained when the solution was treated by ultrasonic sound immediately after the addition of NaOH. The $SnO_2$ nanosheets prepared by means of solution reduction under the ultrasonic treatment, and subsequent oxidation at $600^{\circ}C$ showed a high level of gas sensitivity to $C_2H_5OH$ and $CH_3COCH_3$.

Keywords

References

  1. N. Yamazoe, Sens. Actuators B, 5, 7 (1991) https://doi.org/10.1016/0925-4005(91)80213-4
  2. Y. Shimizu, A. Jono, T. Hyodo and M. Egashira, Sens. Actuators B, 108, 56 (2005) https://doi.org/10.1016/j.snb.2004.10.047
  3. B. -K. Kim and S. -D. Choi, Sens. Actuators B, 98, 239 (2004) https://doi.org/10.1016/j.snb.2003.10.023
  4. A. Kolmakov, Y. Zhang, G. Cheng and M. Moskovits Adv. Mater. 15, 997 (2003) https://doi.org/10.1002/adma.200304889
  5. P. -S. Cho, K. -W. Kim and J. -H. Lee, J. Electroceram. 17, 975 (2006) https://doi.org/10.1007/s10832-006-8146-7
  6. J. Kong, N. R. Franklin, C. Zhou, M. G. Chapline, S. Peng, K. Cho and H. Dai, Science, 287, 622 (2000) https://doi.org/10.1126/science.287.5453.622
  7. E. Comini, G. Faglia, G. Sberveglieri, Z. Pan and Z. L. Wang, Appl. Phys. Lett., 81, 1869 (2002) https://doi.org/10.1063/1.1504867
  8. C. S. Moom, H, R, Kim, G. Aucherlonie, J. Drennan and J. H. Lee, Sens. Actuators B, 131, 556 (2008) https://doi.org/10.1016/j.snb.2007.12.040
  9. G. -W. Yang and H. Li, Mater. Lett., 62, 2189 (2008) https://doi.org/10.1016/j.matlet.2007.11.046
  10. Q. Xiao., S. Huangb, J. Zhang, C. Xiao and X. Tan, J. Alloys Comp., 459, L18 (2008) https://doi.org/10.1016/j.jallcom.2007.05.026
  11. S. Bhattacharyya and A. Gedanken, Micro-porous and Mesoporous Materials, 110, 553 (2008) https://doi.org/10.1016/j.micromeso.2007.06.053
  12. S. Wang, S. Xie, H. Li, S. Yan, K. Fan and M. Qiao, Chem. Commun., p. 507 (2005) https://doi.org/10.1039/b414913k

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