DOI QR코드

DOI QR Code

Fabrication of SiCf/SiC Composites using an Electrophoretic Deposition

  • Lee, Jong-Hyun (School of Materials Science and Engineering, Yeungnam University) ;
  • Gil, Gun-Young (School of Materials Science and Engineering, Yeungnam University) ;
  • Yoon, Dang-Hyok (School of Materials Science and Engineering, Yeungnam University)
  • Published : 2009.09.30

Abstract

Continuous SiC fiber-reinforced SiC composites ($SiC_f$/SiC) were fabricated by electrophoretic deposition (EPD). Nine types of slurries with different powder contents, binder resin amounts and slurry pH were deposited on Tyranno$^{TM}$-SA fabrics by EPD at 135 V for ten minutes to determine the optimal conditions. Further EPD using the optimum slurry conditions was performed on fabrics with four different pyrolitic carbon (PyC) thicknesses. The density of the hot-pressed composites decreased with increasing PyC thickness due to the difficulty of infiltrating the slurry into the narrow gaps between the fibers. On the other hand, the mechanical strength increased with increasing PyC thickness despite the decrease in density, which was explained by the enhanced crack deflection with increasing PyC thickness. The $SiC_f$/SiC composites showed the highest density and flexural strength of 94% and 342 MPa, respectively, showing EPD as a feasible method for dense $SiC_f$/SiC fabrication.

Keywords

References

  1. S.J. Dapkunas, “Ceramic Heat Exchangers,” Am. Ceram. Soc. Bull., 67 388-91 (1988)
  2. Y. Takeda, “Development of High-Thermal-Conductive SiC Ceramics,” Am. Ceram. Soc. Bull., 67 1961-63 (1988)
  3. B. Riccardi, P. Fenici, A.F. Rebelo, L. Giancarli, G.L. Marois, and E. Philippe, “Status of the European R&D Activities on $SiC_f/SiC$ Composites for Fusion Reactors,” Fusion Eng. Des., 51-52 11-22 (2000) https://doi.org/10.1016/S0920-3796(00)00311-2
  4. B. Riccardi, L. Giancarli, A. Hasegawa, Y. Katoh, A. Kohyama, R.H. Jones, and L.L. Snead, “Issues and Advances in $SiC_f/SiC$ Composites Development for Fusion Reactors,” J. Nucl. Mater., 329-333 56-65 (2004) https://doi.org/10.1016/j.jnucmat.2004.04.002
  5. R.J. Kerans and T.A. Parthasarathy, “Crack Deflection in Ceramic Composites and Fiber Coating Design Criteria,” Compos. Part A, 30 521-24 (1999) https://doi.org/10.1016/S1359-835X(98)00144-4
  6. R. Yamada, T. Taguvhi, and N. Igawa, “Mechanical and Thermal Properties of 2D and 3D SiC/SiC Composites,” J. Nucl. Mater., 283-287 574-78 (2000) https://doi.org/10.1016/S0022-3115(00)00144-6
  7. A. Ortona, A. Donato, G. Filacchioni, U.D. Angelis, A.L. Barbera, C.A. Nannetti, B. Riccardi, and J. Yeatman, “ $SiC-SiC_f$ CMC Manufacturing by Hybrid CVI-PIP Techniques: Process Optimasation,” Fusion Eng. Des., 51-52 159-63 (2000) https://doi.org/10.1016/S0920-3796(00)00310-0
  8. Y. Katoh, S.M. Dong, and A. Kohyama, “Thermo-mechanical Properties and Microstructure of Silicon Carbide Composites Fabricated by Nano-infiltrated Transient Eutectoid Process,” Fusion Eng. Des., 61-62 723-31 (2002) https://doi.org/10.1016/S0920-3796(02)00180-1
  9. S. Dong, Y. Katoh, and A. Kohyama, “Preparation of SiC/ SiC Composites by Hot Pressing, Using Tyranno-SA Fibers as Reinforcement,” J. Am. Ceram. Soc., 86 [1] 26-32 (2003) https://doi.org/10.1111/j.1151-2916.2003.tb03272.x
  10. K. Shimoda, J.S. Park, T. Hinoki, and A. Kohyama, “Influence of Pyrolytic Carbon Interface Thickness on Microstructure and Mechanical Properties of SiC/SiC Composites by NITE Process,” Ceram. Sci. Technol., 68 98-105 (2008) https://doi.org/10.1016/j.compscitech.2007.05.037
  11. T. Ishikawa, Y. Kohtoku, K. Kumagawa, T. Yamamura, and T. Nagasawa, “High-Strength Alkai-Resistant Sintered SiC Fibre Stable to $2,200^{\circ}C$,” Nature, 391 773-75 (1998) https://doi.org/10.1038/35820
  12. L. Besra, and M. Liu, “A Review on Fundamentals and Applications of Electrophoretic Deposition (EPD),” Prog. Mater. Sci., 52 1-61 (2007) https://doi.org/10.1016/j.pmatsci.2006.07.001
  13. S. Novak, K. Rade, K. König, and A.R. Boccaccini, “Electrophoretic Deposition in the Production of SiC/SiC Composites for Fusion Reactor Applications,” J. Eur. Ceram. Soc., 28 2801-07 (2008) https://doi.org/10.1016/j.jeurceramsoc.2008.04.004
  14. K. Yoshida, K. Matsukawa, M. Imai, and T. Yano, “Formation of Carbon Coating on SiC Fiber for Two-Dimensional $SiC_f/SiC$ Composites by Electrophoretic Deposition,” Mat. Sci. Eng. B, 161 188-92 (2009) https://doi.org/10.1016/j.mseb.2008.11.032
  15. K. Yoshida, K. Matsukawa, and T. Yano, “Microstructure and Mechanical Properties of Silicon Carbide Fiber-Reinforced Silicon Carbide Composite Fabricated by Electrophoretic Deposition and Hot-Pressing,” J. Nucl. Mater., 386-388 643-46 (2009) https://doi.org/10.1016/j.jnucmat.2008.12.314
  16. J.H. Lee, P. Yonathan, D.H. Yoon, W.J. Kim, and J.Y. Park, “Dispersion Stability and Its Effect on Tape Casting of Solvent-Based SiC Slurries,” J. Ceram. Proc. Res., 10 301-07 (2009)

Cited by

  1. /SiC Composites vol.48, pp.5, 2011, https://doi.org/10.4191/kcers.2011.48.5.335
  2. Formation of a Carbon Interphase Layer on SiC Fibers Using Electrophoretic Deposition and Infiltration Methods vol.52, pp.4, 2015, https://doi.org/10.4191/kcers.2015.52.4.284
  3. Electrophoretic (Infiltration) Deposition of Thick Conductive Fiber Preforms vol.162, pp.11, 2015, https://doi.org/10.1149/2.0141511jes
  4. Stability and electrophoretic deposition of nano-SiC assisted by PEI pp.1532-2351, 2019, https://doi.org/10.1080/01932691.2018.1535978