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Fabrication and Properties of SiC Candle Filter by Vacuum Extrusion and Ramming Process (II)

진공 압출성형 및 래밍성형 공정에 의한 탄화규소 캔들 필터 제조 및 특성 (II)

  • Han, In-Sub (Reaction and Separation Materials Research Center, Korea Institute of Energy Research (KIER)) ;
  • Seo, Doo-Won (Reaction and Separation Materials Research Center, Korea Institute of Energy Research (KIER)) ;
  • Kim, Se-Young (Reaction and Separation Materials Research Center, Korea Institute of Energy Research (KIER)) ;
  • Hong, Ki-Seog (Reaction and Separation Materials Research Center, Korea Institute of Energy Research (KIER)) ;
  • Woo, Sang-Kuk (Reaction and Separation Materials Research Center, Korea Institute of Energy Research (KIER)) ;
  • Kim, Young-Wook (Department of Materials Science Engineering, the University of Seoul)
  • 한인섭 (한국에너지기술연구원 반응분리소재연구센터) ;
  • 서두원 (한국에너지기술연구원 반응분리소재연구센터) ;
  • 김세영 (한국에너지기술연구원 반응분리소재연구센터) ;
  • 홍기석 (한국에너지기술연구원 반응분리소재연구센터) ;
  • 우상국 (한국에너지기술연구원 반응분리소재연구센터) ;
  • 김영욱 (서울시립대학교 신소재공학과)
  • Received : 2010.09.29
  • Accepted : 2010.10.29
  • Published : 2010.11.30

Abstract

Porous SiC candle filter preforms were fabricated by extrusion and ramming process. To fabricate SiC candle filter preform, commercially available F180 mesh ($85\;{\mu}m$) $\alpha$-SiC powder and $44\;{\mu}m$ mullite, $CaCO_3$ powder were used as the starting materials. The candle type preforms were fabricated by vacuum extrusion and ramming process, and sintered at $1400^{\circ}C$ 2 h in air atmosphere. Corrosion test of the sintered candle filter specimens as forming method was performed at $600^{\circ}C$ for 2,400 h in simulated IGCC syngas atmosphere. The effect of forming method on mechanical properties, pore distribution, microstructure and crystalline phase was investigated.

Keywords

References

  1. Ohzawa Y., Nomura K., and Sugiyama K., “Relation between Porosity and Pore Size or Pressure Drop of Fibrous SiC Filter Prepared from Carbonized Cellulose-Powder Preforms,” Mater. Sci. and Eng., A255 33-8 (1998).
  2. Stringer J. and Leitch A. J., “Ceramic Candle Filter Performance at the Gremethopre (UK) Pressurized Fluidized Bed Combustior,” J. Eng. Gas Turb. Power-T ASME, 114 371-79 (1992). https://doi.org/10.1115/1.2906601
  3. Hajek S. and Peukert W., “Experimental Investigations with Ceramic High-temperature Filter Media,” Filtration & Separation, 34 [1] 29-37 (1996).
  4. Chaudhuri M., Verma S. R., and Gupta A., “Performance Evaluation of Ceramic Filter Candles,” J. Environ. Eng., 120 1646-51 (1994). https://doi.org/10.1061/(ASCE)0733-9372(1994)120:6(1646)
  5. Judkins R. R., Stinton D. P., and DeVan J. H., “A Review of the Efficacy of Silicon Carbide Hot Gas Filters in Coal Gasification and Pressurized Fluidized Bed Combustion Environments,” Trans. ASME, 118 500-6 (1996).
  6. M. A. Alvin, “Filter Component Assessment - Ceramic Candles-,” pp.8-24, Final Report, DOE/NETL Contract No. DE-AC21-94MC31147, 2004.
  7. M. K. Shin, I. S. Han, D. W. Seo, S. Y. Kim, S. K. Woo, S. W. Lee, and Y.-W. Kim, “Fabrication and Properties of the SiC Candle Filter by Vacuum Extrusion and Ramming Process(in Korean),” J. Kor. Ceram. Soc., 46 [6] 662-67 (2009). https://doi.org/10.4191/KCERS.2009.46.6.662
  8. R. A. Newby, T. E. Lippert and M. A. Alvin, G. J. Burck, and Z. N. Sanjana, “Status of Westinghouse Hot Gas Filters for Coal and Biomass Power System,” J. Eng. Gas Turb. Power-T ASME, 121 401-8 (1999). https://doi.org/10.1115/1.2818487
  9. R. Westerheide, J. Adler, A. Walch, W. Volker, H. Buhl, and D. Fister, “High Temperature Gas Cleaning,” pp. 255-287, Vol. II, Dittler A., Hemmer G. and Kasper G., (Ed.), Institut fr Mechanische Verfahrenstechnik und Mechanik der Universitt Karlsruhe, Germany, 1990.
  10. P. Pastila, V. Helanti, A. P. Nikkila, and T. Mantyla, “Environmental Effects on Microstructure and Strength of SiCbased Hot Gas Filters,” J. Eur. Ceram. Soc., 21 [9] 1261-68 (2001). https://doi.org/10.1016/S0955-2219(00)00326-5

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