DOI QR코드

DOI QR Code

Determination of the Size Distribution of Magnetite Nanoparticles from Magnetic Measurements

  • 투고 : 2011.10.04
  • 심사 : 2011.10.26
  • 발행 : 2011.12.31

초록

Particle size distributions in 10 nm magnetite ferrofluids are analyzed based on both dc and ac magnetic measurements. Modified log-normal distributions are used for fitting the experimental results, which allows for a proper account of the narrow distributions. The calculated average particle sizes are in good agreement with the TEM results. However the ac method gives a much narrower distribution width than that of the dc magnetization curve fit. The proposed measurements combined with the analysis methods are useful for the characterization of ferrofluids being considered for biomedical applications.

키워드

참고문헌

  1. K. M. Krishnan, IEEE Trans. Magn. 46, 2523 (2010). https://doi.org/10.1109/TMAG.2010.2046907
  2. S. H. Chung, A. Hoffmann, S. D. Bader, C. Liu, B. Kay, L. Makowski, and L. Chen, Appl. Phys. Lett. 85, 2971 (2004). https://doi.org/10.1063/1.1801687
  3. Y. Bao, A. B. Pakhomov, and K. M. Krishnan, J. Appl. Phys. 99, 08H107 (2006). https://doi.org/10.1063/1.2172203
  4. Joan Connolly and Timothy G. St. Pierre, J. Magn. Magn. Mater. 225, 156 (2001). https://doi.org/10.1016/S0304-8853(00)01245-2
  5. R. Hergt, R. Hiergeist, M. Zeisberger, G. Glockl, W. Weitschies, L. P. Lamirez, I. Hilger, and W. A. Kaiser, J. Magn. Magn. Mater. 280, 358 (2004). https://doi.org/10.1016/j.jmmm.2004.03.034
  6. M. I. Shliomis, Sov. Phys.-Usp. 17, 153 (1974). https://doi.org/10.1070/PU1974v017n02ABEH004332
  7. W. F. Brown, J. Appl. Phys. 34, 1319 (1963). https://doi.org/10.1063/1.1729489
  8. P. Debye, Polar Molecules, Chemical Catalog Company, New York (1929).
  9. R. W. Chantrell, J. Popplewell, and S. W. Charles, IEEE Trans. Magn. 14, 975 (1978). https://doi.org/10.1109/TMAG.1978.1059918
  10. S.-H. Yoon, M. Gonzales-Weimuller, Y.-C. Lee, and Kannan M. Krishnan, J. Appl. Phys. 105, 07B507 (2009). https://doi.org/10.1063/1.3068527
  11. P. C. Fannin, B. K. P. Scaife, and S. W. Charles, J. Magn. Magn. Mater. 65, 279 (1987). https://doi.org/10.1016/0304-8853(87)90051-5
  12. R. E. Rosensweig, J. Magn. Magn. Mater. 252, 370 (2002). https://doi.org/10.1016/S0304-8853(02)00706-0
  13. M. Gonzales and K. M. Krishnan, J. Magn. Magn. Mater. 293, 265 (2006).
  14. T. Hyeon, S. S. Lee, J.-N. Park, Y.-H. Chung, and H. B. Na, J. Am. Chem. Soc. 123, 12798 (2001). https://doi.org/10.1021/ja016812s
  15. A. G. Loca, M. P. Morales, and C. J. Serna, IEEE Trans. Magn. 42, 3025 (2006). https://doi.org/10.1109/TMAG.2006.880111
  16. P. C. Fannin, B. K. P. Scaife, and S. W. Charles, J. Phys. E: Sci. Instrum. 19, 238 (1986). https://doi.org/10.1088/0022-3735/19/3/018
  17. P. C. Fannin, B. K. P. Scaife, and S. W. Charles, J. Magn. Magn. Mater. 72, 95 (1988). https://doi.org/10.1016/0304-8853(88)90276-4
  18. E. P. Wohlfarth, Ferromagnetic Materials, North-Holland, Amsterdam (1982).
  19. S.-H. Yoon, J. Korean Phys. Soc. 54, 163 (2009). https://doi.org/10.3938/jkps.54.163
  20. P. C. Fannin and S. W. Charles, J. Phys. D: Appl. Phys. 22, 187 (1989). https://doi.org/10.1088/0022-3727/22/1/027

피인용 문헌

  1. On variations in size distributions of particles and aggregates upon dilution of magnetic fluids vol.79, pp.1, 2017, https://doi.org/10.1134/S1061933X17010033
  2. On the temperature dependence of ferrofluid susceptibility vol.185, pp.2100-014X, 2018, https://doi.org/10.1051/epjconf/201818509011