DOI QR코드

DOI QR Code

Surface Characteristics of the Ground Zirconia

연삭된 지르코니아의 표면 특성

  • Kim, Sa-Hak (Department of Dental Laboratory Technology, Dong-U College)
  • Received : 2011.10.31
  • Accepted : 2011.12.28
  • Published : 2011.12.30

Abstract

Purpose: This study was conducted to examine the phase transition according to the zirconia surface treatment. Methods: The specimens were divided to four groups. The first group was sintered at $1,500^{\circ}C$ and ground; the second group was sintered at $700^{\circ}C$, ground, and sintered at $1,500^{\circ}C$; the third group was sintered at $1,500^{\circ}C$, ground, and $110{\mu}m$-sandblasted; and the fourth group was sintered at $1,500^{\circ}C$, ground, $110{\mu}m$-sandblasted, treated with 9.5% hydrofluoric acid, and ultrasonic cleaner-washed for two minutes. The monoclinic fractions were measured, and the surface was observed via SEM. Results: The monoclinic fraction was $0.13{\pm}0.19%$ in the control group Zr1, $1.91{\pm}0.15%$ in the experimental group Zr2, $7.71{\pm}0.34%$ in Zr3, and $8.39{\pm}0.25%$ in Zr4. On the surface, the phase transition hardly occurred in the control group Zr1, but it increasingly occurred in the experimental groups Zr3 and Zr4. Conclusion: The monoclinic fraction was high in the experimental groups Zr3 and Zr4. The phase transition did not occur in the control group, but increasingly occurred in the experimental groups.

Keywords

References

  1. 김사학. 지르코니아 포세린의 전단결합강도. 대한치과기공학회지, 33(1), 1-8, 2011.
  2. 박항민, 정인성. 지르코니아 코어의 표면처리방법이 열가압 세라믹과의 전단결합강도에 미치는 영향. 대한치과기공학회지, 31(2), 23-29, 2009.
  3. Aboushelib MN, Matinlinna JP, Salamdo Z, Ounsa H. Innovations in bonding to zirconia-based materials: Part I. Dent Mater, 24: 1268-1272, 2008. https://doi.org/10.1016/j.dental.2008.02.010
  4. Amaral R, O¨zcan M, Valandro LF, Balducci I, Bottino MA. Effect of conditioning methods on the microtensile bond strength of phosphate monomer-based cement on zirconia ceramic in and aged conditions. J Biomed Mater Res, Appl Biomater, 85B, 1-9, 2008. https://doi.org/10.1002/jbm.b.30908
  5. Bona AD, Anusavice KJ. Microstructure, composition, and etching topography of dental ceramics. Int J Prosthodont, 15, 159- 167, 2002.
  6. Christel P, Meunier A, Heller M, Torre JP, Peille CN. Mechanical properties and short-term in-vivo evalution of yttrium-oxidepartially- stabilized zirconia. J Biomed Mater Res, 23, 45-61, 1989. https://doi.org/10.1002/jbm.820230105
  7. DeJager N, Pallav P, Feilzer AJ. The influence of design parameters on the FEA-determined stress distribution in CAD-CAM produced all-ceramic dental crowns. Dent mater, 21, 242-251, 2005. https://doi.org/10.1016/j.dental.2004.03.013
  8. Denry IL, Kelly JR. State of the art of zirconia for dental applications. Dent Mater, 24, 299-307, 2008. https://doi.org/10.1016/j.dental.2007.05.007
  9. Garvie RC, Hannink RH, Pascoe RT. Ceramic steel. Nature, 258, 703-704, 1975. https://doi.org/10.1038/258703a0
  10. Gupta TK, Lange FF, Bechtold JH. Effect of stress induced phase transformatuin on the properties on the properties of polycrystalline zirconia-containing trtragonal phase. J Mater Sci, 13, 1464-1470, 1978. https://doi.org/10.1007/BF00553200
  11. Kern M, Wegner SM. Bonding to zirconia ceramic : adhesion methods and their durability. Dent Mater, 14, 64-71, 1998. https://doi.org/10.1016/S0109-5641(98)00011-6
  12. Larsson C, von Steyem PV, Sunzel B, Nilner K. All-ceramic two- and five-unit implant supported reconstructions. A randomized, prospective clinical trial, Swed Dent J, 30, 45-53, 2006.
  13. Luthardt R, Weber A, Rudolph H, Schone C, Quaas S, Walter M. Design and production of dental prosthetic restorations: basic research on dental CAD/CAM technology. Int J Comput Dent, 5(2-3), 165-176, 2002.
  14. Porter DL, Heuer AH. Mechanism of toughening partially stabilized zirconia(PSZ). J Am Ceram Soc, 60, 183-218, 1977. https://doi.org/10.1111/j.1151-2916.1977.tb15509.x
  15. Piconi C, Maccauro G. Review zirconia as a ceramic biomaterial. Biomaterials, 20, 1-25, 1999. https://doi.org/10.1016/S0142-9612(98)00010-6
  16. Wohlwend A, Studer S, Scharer P. The zirconium oxide abutment: an all-ceramic abutment for the esthetic improvement of implant superstructures. Quintessence Dent Technol, 1, 63-74, 1997.