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Quality Characteristics of Fruit Spirits from a Copper Distillation Apparatus

동증류기를 이용한 과실증류주의 품질 특성

  • Cho, Ho-Cheol (Dept. of Convergence Industry, Seoul Venture University) ;
  • Kang, Soon Ah (Dept. of Conversing Technology, Graduate School of Venture, Hoseo University) ;
  • Choi, Sung-Inn (Dept. of Convergence Industry, Seoul Venture University) ;
  • Cheong, Chul (Dept. of Convergence Industry, Seoul Venture University)
  • 조호철 (서울벤처대학원대학교 융합산업학과) ;
  • 강순아 (호서대학교 벤처전문대학원 융합공학과) ;
  • 최성인 (서울벤처대학원대학교 융합산업학과) ;
  • 정철 (서울벤처대학원대학교 융합산업학과)
  • Received : 2012.10.29
  • Accepted : 2013.04.08
  • Published : 2013.05.31

Abstract

The objective of this study was to investigate the quality characteristics of spirits derived from fruit using copper distillation equipment. First, optimal yeast strains were chosen through a fermentation test on raw materials (apples, mandarins and rowanberries). The normal fermentation condition for rowanberries observed at a rowanberry concentration of 8% during mashing included chaptalization with sugar to increase the alcohol content. During the mashing, fruits were fermented and distilled through one of three different types of distillation apparatuses (pot distiller, vacuum distiller, or multistage distiller made of copper). The results revealed that the type of apparatus used affects the content of alcohol and flavor components. The distilled spirits prepared through a copper multistage distiller had a much higher tendency to retain components of fruit aromas such as ethyl acetate and provided higher yields than spirits prepared with a pot distiller or vacuum distiller. Thus, the copper multistage distiller apparatus can be applied to positively influence the taste and flavor of fruit distilled spirits by enhancing fruit aromas, removing impurities such as sulfur components and enhancing yields.

과실을 이용한 증류주 개발에 있어서 국내에서 생산량이 많고 과잉생산으로 인한 잉여과실 발생빈도가 높은 사과와 감귤을 선정하였으며, 외국에서 증류주 제조에 많이 사용하고 국내에 많이 자생하는 마가목 열매를 원료로 선정하여 본 연구를 수행하였다. 각 원료의 발효특성에 따라 맞춤형 효모를 선정하였고, 선정된 효모를 이용하여 발효한 술덧을 동재질의 상압다단식 증류기와 스테인리스 재질의 상압단식 증류기 및 감압단식증류기 등으로 각각 증류한 증류주의 주요 향기성분과 증류효율 등을 비교 평가하였다. 또한 상기 증류주의 품질평가를 위해 4개월 숙성 후 관능평가를 실시하였다. 연구결과 사과와 감귤의 경우 원료 사용비율에 관계없이 발효가 원활히 진행되었으나 마가목 열매의 경우 원료사용비율이 10 w/v% 이상일 경우 발효가 되지 않거나 미미하였으며, 사용비율이 8 w/v% 이하일 때에는 원활한 발효가 진행되었다. 원료별, 증류방식별로 초류, 본류, 후류로 나누어 증류한 증류주의 증류효율을 검토한 결과 과실 원료 차이에 따른 증류주의 수율 차이는 적었지만, 증류효율 면에서는 상압다단식 증류기, 상압단식, 감압단식 순으로 높게 나타났다. 과실증류주의 주요 향기성분 분석결과 증류방식별 다소의 차이를 나타내었으나 모든 원료에서 동재질의 상압다단식증류 방식에 의해 제조된 시제품이 스테인리스 재질의 상압단식 및 감압단식방식에 의해 제조된 증류주에 비해 아로마가 풍부한 것으로 나타났다. 결론적으로 사용된 원료에 관계없이 증류수율, 작업능률 및 품질측면에서 동재질의 상압다단식증류방식이 스테인리스 재질의 단식 또는 감압증류방식보다는 증류주제조에 더 적합한 것으로 나타났다. 쌀을 이용한 증류주 제조에만 국한되어 있는 국내 증류주시장을 고려하면 과실을 이용한 유럽스타일의 증류주 제조, 특히 마가목 열매를 이용한 과실증류주 상품화 기술은 향후 FTA 시대를 맞아 시장 다변화 및 우리술 경쟁력 강화에 기여할 것으로 보인다.

Keywords

References

  1. Lee HK, Choi YS, Chung EH. 1989. Higher alcohols composition in Korean alcoholic beverages. Kor J Food Hygiene 4: 257-262.
  2. Lee KH. 1977. Studies on fine spirits aging. [Part I] On the aptitude of the Korean oak varieties as barrels for aging apple fine spirits. J Korean Agric Chem Soc 20: 66-80.
  3. Min YK, Yun HS, Jeong HS. 1994. Studies on the distillation operation of Baikha-ju. Agric Chem Biotechnol 37: 9-13.
  4. Lee DS, Park HS, Kim K, Lee TS, Noh BS. 1994. Physicochemical characteristics of Korean folk sojues. Korean J Food Sci Technol 26: 649-654.
  5. In HY, Lee TS, Lee DS, Noh BS. 1995. Volatile components and fusel oils of sojues and mashes brewed by Korean traditional method. Korean J Food Sci Technol 27: 235-240.
  6. Lee DS, Park HS, Kim K, Lee TS, Noh BS. 1994. Determination and multivariate analysis of flavour components in the Korean folk sojues using GC-MS. Korean J Food Sci Technol 26: 750-758.
  7. Jang JH. 1989. The history of Korean alcoholic liqours. Korean J Dietary Culture 4: 271-274.
  8. Choi JI, Hong WH. 1999. Recovery of lactic acid by batch distillation with chemical reactions using ion exchange resin. J Chem Eng J pn 32: 184-189. https://doi.org/10.1252/jcej.32.184
  9. Bae KH, Shin KS, Ryu HY, Kwon CS, Shon HY. 2007. Identification and fermentation characteristics of lactic bacteria from the fermentation broth of Korean traditional liquor, Andong-Soju. Kor J Microbiol Biotechnol 35: 310-315.
  10. Kim HR, Ahn BH. 2001. Research trend of Korean traditional alcoholic beverage. 2001. Food Industry and Nutrition 6(3): 5-10.
  11. Bae KH, Ryu HY, Kwun IS, Kwon CS, Shon HY. 2007. Optimization of thickness and maturation period of Andong-Soju nuruk for fermentation of Andong-Soju. Kor J Microbiol Biotechnol 35: 231-237.
  12. Bae SM, Jung SY, Jung IS, Ko HJ, Kim TY. 2003. Effect of the amount of water on the yield and flavor of Korean distilled liquor based on rice and corn starch. J East Asian Soc Dietary Life 13: 439-446.
  13. Ryu. LH, Kim YM. 2002. Esterification of alcohols with organic acids during distilled spirit distillation. Korean J Food & Nutr 15: 259-299.
  14. Bae YD. 2006. The history and meaning of the production and consumption of Andong Soju. Local History and Culture 9: 375-413. https://doi.org/10.17068/lhc.2006.11.9.2.375
  15. Hong Y, Park SK, Choi EH. 1999. Flavor characteristics of Korean traditional distilled liquors produced by co-culture Saccharomyces and Hansenula. Kor J App Microbiol Biotechnol 27: 236-245.
  16. Kang CS, Hong JU, Chung KT. 1987. The changes of fusel oil contents during apple aging-I. Res Bull Inst Agr Sci Tech Kyungbook Natl Univ 4: 75-82.
  17. Kang CS, Han YK, Hong JU, Chung KT. 1987. The changes of fusel oil contents during apple aging-II. Res Bull Inst Agr Sci Tech Kyungbook Natl Univ 4: 83-90.
  18. Cheong C, Cho SK. 2010. The research trend and technological improvement subject of Korean distilled spirit. KARC, Korea. p 1-123.
  19. Yi HC, Moon SH, Park JS, Jung JW, Hwang KT. 2010. Volatile compounds in liquor distilled from mash produced using koji or nuruk under reduced or atmospheric pressure. J Korean Soc Food Sci Nutr 39: 880-886. https://doi.org/10.3746/jkfn.2010.39.6.880
  20. Min YK, Yun HS, Jeong HS, Jang YS. 1992. Changes in compositions of liquor fractions distilled from Samil-ju with various distillation conditions. Korean J Food Sci Technol 24: 440-446.
  21. Lee MK, Lee HY, Lee JH, Oh JS, Chio GP, Kim JH, Kim JD. 2002. Anticancer effect of Sorbus commixta Hedl extracts. Korean J Medicinal Crop Sci 10: 403-408.
  22. Chung BH, Lee HY, Kim JH, Kim NY, Lee SY, Choi JT, Kim JH, Kim JD. 2003. Effect of fruit extracts from Sorbus commixta Hedl. on the lipid metabolism in rats. Korean J Medicinal Crop Sci 11: 143-147.
  23. NTS Liquors Licence Aid Center. 2008. Regulations of analysis in alcoholic beverages. p 1-68.
  24. Goelles A. 2000. Edel Braende. 2th ed. Leopold Stocker Publisher, Graz-Stuttgart. p 70.

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